tert-butyldiphenylsilyl 2,4-di-O-benzyl-β-D-mannopyranosyl-(1→4)-3,6-di-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-glucopyranoside

Base Information

• Chemical Name: tert-butyldiphenylsilyl 2,4-di-O-benzyl-β-D-mannopyranosyl-(1→4)-3,6-di-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-glucopyranoside
• CAS No.: 1392318-12-5
• Molecular Formula: C₅₈H₆₄Cl₃NO₁₁Si
• Molecular Weight: 1085.59
• Mol file: 1392318-12-5.mol

Synonyms:tert-butyldiphenylsilyl 2,4-di-O-benzyl-β-D-mannopyranosyl-(1→4)-3,6-di-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-glucopyranoside

Chemical Property of tert-butyldiphenylsilyl 2,4-di-O-benzyl-β-D-mannopyranosyl-(1→4)-3,6-di-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-glucopyranoside

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of tert-butyldiphenylsilyl 2,4-di-O-benzyl-β-D-mannopyranosyl-(1→4)-3,6-di-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-glucopyranoside

There total 1 articles about tert-butyldiphenylsilyl 2,4-di-O-benzyl-β-D-mannopyranosyl-(1→4)-3,6-di-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C66H72Cl3NO12Si → tert-butyldiphenylsilyl 2,4-di-O-benzyl-β-D-mannopyranosyl-(1→4)-3,6-di-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-glucopyranoside (1392318-12-5)

Guidance literature:

With trifluoroacetic acid; In dichloromethane; water; at -10 ℃; for 0.75h;

DOI:10.1021/jo3010155

Reference yield: 85.0%

tert-butyldiphenylsilyl 2,4-di-O-benzyl-β-D-mannopyranosyl-(1→4)-3,6-di-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-glucopyranoside (1392318-12-5) + 2-O-acetyl-3,4,6-tri-O-benzyl-α/β-D-mannopyranosyl fluoride (169106-94-9) → C116H124Cl3NO23Si

Guidance literature:

With (η(5)-cyclopentadienyl)zirconium dichloride radical; silver perchlorate; In dichloromethane; at -40 - -15 ℃; for 1.5h; Molecular sieve; Inert atmosphere;

DOI:10.1021/jo3010155