1-Benzyl-aziridine-2-carboxylic acid benzyl-((Z)-6-benzyloxy-hex-3-enyl)-amide

Base Information

• Chemical Name: 1-Benzyl-aziridine-2-carboxylic acid benzyl-((Z)-6-benzyloxy-hex-3-enyl)-amide
• CAS No.: 133627-49-3
• Molecular Formula: C₃₀H₃₄N₂O₂
• Molecular Weight: 454.612

Synonyms:1-Benzyl-aziridine-2-carboxylic acid benzyl-((Z)-6-benzyloxy-hex-3-enyl)-amide

Chemical Property of 1-Benzyl-aziridine-2-carboxylic acid benzyl-((Z)-6-benzyloxy-hex-3-enyl)-amide

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Technology Process of 1-Benzyl-aziridine-2-carboxylic acid benzyl-((Z)-6-benzyloxy-hex-3-enyl)-amide

There total 3 articles about 1-Benzyl-aziridine-2-carboxylic acid benzyl-((Z)-6-benzyloxy-hex-3-enyl)-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methyl 1-benzylaziridine-2-carboxylate (21384-53-2,31907-91-2,196965-62-5) → 1-Benzyl-aziridine-2-carboxylic acid benzyl-((Z)-6-benzyloxy-hex-3-enyl)-amide (133627-49-3)

Guidance literature:

Multi-step reaction with 3 steps

1: KOTMS / tetrahydrofuran

2: CH₂Cl₂

3: DMAP

With dmap; potassium trimethylsilonate; In tetrahydrofuran; dichloromethane;

DOI:10.1021/jo00010a006

Reference yield:

Potassium; 1-benzyl-aziridine-2-carboxylate → 1-Benzyl-aziridine-2-carboxylic acid benzyl-((Z)-6-benzyloxy-hex-3-enyl)-amide (133627-49-3)

Guidance literature:

Multi-step reaction with 2 steps

1: CH₂Cl₂

2: DMAP

With dmap; In dichloromethane;

DOI:10.1021/jo00010a006

Reference yield:

C15H19NO3 + Benzyl-((Z)-6-benzyloxy-hex-3-enyl)-amine (133627-48-2) → 1-Benzyl-aziridine-2-carboxylic acid benzyl-((Z)-6-benzyloxy-hex-3-enyl)-amide (133627-49-3)

Guidance literature:

With dmap; Yield given;

DOI:10.1021/jo00010a006

upstream raw materials:

Benzyl-((Z)-6-benzyloxy-hex-3-enyl)-amine

methyl 1-benzylaziridine-2-carboxylate

Downstream raw materials:

(3R,3aS,7aR)-1-Benzyl-6-(toluene-4-sulfonyl)-3-((E)-4-trimethylsilanyl-but-2-enyl)-octahydro-pyrrolo[2,3-c]pyridin-7-one

(3R,3aS,7aR)-1-Benzyl-6-(toluene-4-sulfonyl)-3-((E)-4-trimethylsilanyl-but-2-enyl)-octahydro-pyrrolo[2,3-c]pyridin-7-ol

Acetic acid 1-((3R,3aS,7aR)-1,6-dibenzyl-7-oxo-octahydro-pyrrolo[2,3-c]pyridin-3-ylmethyl)-allyl ester

(1S,4S,7S,8R)-6-Benzyl-11-(toluene-4-sulfonyl)-2-vinyl-6,11-diaza-tricyclo[5.4.0.0^4,8]undecane

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