methyl hydrogen (benzyloxy)((4R,5S)-2,2-dimethyl-5-vinyl-1,3-dioxolan-4-yl)methylphosphonate

Base Information

Chemical Name:methyl hydrogen (benzyloxy)((4R,5S)-2,2-dimethyl-5-vinyl-1,3-dioxolan-4-yl)methylphosphonate
CAS No.:952716-26-6
Molecular Formula:C₁₆H₂₃O₆P
Molecular Weight:342.329
Hs Code.:

Synonyms:methyl hydrogen (benzyloxy)((4R,5S)-2,2-dimethyl-5-vinyl-1,3-dioxolan-4-yl)methylphosphonate

Suppliers and Price of methyl hydrogen (benzyloxy)((4R,5S)-2,2-dimethyl-5-vinyl-1,3-dioxolan-4-yl)methylphosphonate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of methyl hydrogen (benzyloxy)((4R,5S)-2,2-dimethyl-5-vinyl-1,3-dioxolan-4-yl)methylphosphonate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of methyl hydrogen (benzyloxy)((4R,5S)-2,2-dimethyl-5-vinyl-1,3-dioxolan-4-yl)methylphosphonate

There total 7 articles about methyl hydrogen (benzyloxy)((4R,5S)-2,2-dimethyl-5-vinyl-1,3-dioxolan-4-yl)methylphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 952716-24-4
dimethyl (benzyloxy)((4R,5S)-2,2-dimethyl-5-vinyl-1,3-dioxolan-4-yl)methylphosphonate

: 952716-26-6
methyl hydrogen (benzyloxy)((4R,5S)-2,2-dimethyl-5-vinyl-1,3-dioxolan-4-yl)methylphosphonate

Guidance literature:: With sodium hydroxide; for 7h; Heating;
DOI:10.1016/j.tet.2007.07.032

Reference yield:

: 1058706-86-7
(S,S)-2,2-dimethyl-4-[(tert-butyldimethylsilyloxy)methyl]-5-vinyl-1,3-dioxolane

: 952716-26-6
methyl hydrogen (benzyloxy)((4R,5S)-2,2-dimethyl-5-vinyl-1,3-dioxolan-4-yl)methylphosphonate

Guidance literature:: Multi-step reaction with 3 steps

1: 2.55 g / CH₂Cl₂ / 20 °C

2: 92 percent / Ag₂O / dimethylformamide / 48 h / 20 °C

3: 52 percent / aq. NaOH / 7 h / Heating

With sodium hydroxide; silver(l) oxide; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2007.07.032

Reference yield:

: 952716-22-2
dimethyl hydroxy((4R,5S)-2,2-dimethyl-5-vinyl-1,3-dioxolan-4-yl)methylphosphonate

: 952716-26-6
methyl hydrogen (benzyloxy)((4R,5S)-2,2-dimethyl-5-vinyl-1,3-dioxolan-4-yl)methylphosphonate

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / Ag₂O / dimethylformamide / 48 h / 20 °C

2: 52 percent / aq. NaOH / 7 h / Heating

With sodium hydroxide; silver(l) oxide; In N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2007.07.032