Technology Process of C31H34N8O6
There total 4 articles about C31H34N8O6 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine;
In
N,N-dimethyl-formamide;
at 20 ℃;
for 48h;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: piperidine / dichloromethane / 0.17 h / 20 °C
1.2: 0.17 h / 20 °C
2.1: sodium tetrahydroborate / isopropyl alcohol; water / 1 h / 60 °C
2.2: 48 h / 20 - 80 °C
3.1: triethylamine; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / N,N-dimethyl-formamide / 48 h / 20 °C / Inert atmosphere
With
piperidine; sodium tetrahydroborate; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine;
In
dichloromethane; water; N,N-dimethyl-formamide; isopropyl alcohol;
1.1: Knoevenagel Condensation;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: sodium tetrahydroborate / isopropyl alcohol; water / 1 h / 60 °C
1.2: 48 h / 20 - 80 °C
2.1: triethylamine; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / N,N-dimethyl-formamide / 48 h / 20 °C / Inert atmosphere
With
sodium tetrahydroborate; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine;
In
water; N,N-dimethyl-formamide; isopropyl alcohol;