(2R,3R,4R,5S,6S)-2-(acetoxymethyl)-6-(4-chIoro-3-((5-methyl-6-oxo-1,6-dihvdropyridazin-3-yl)methyl)phenyl)tetrahydro-2H-pyran-3,4.5-triyI triacetate

Base Information

• Chemical Name: (2R,3R,4R,5S,6S)-2-(acetoxymethyl)-6-(4-chIoro-3-((5-methyl-6-oxo-1,6-dihvdropyridazin-3-yl)methyl)phenyl)tetrahydro-2H-pyran-3,4.5-triyI triacetate
• CAS No.: 1259019-52-7
• Molecular Formula: C₂₆H₂₉ClN₂O₁₀
• Molecular Weight: 564.977

Synonyms:(2R,3R,4R,5S,6S)-2-(acetoxymethyl)-6-(4-chIoro-3-((5-methyl-6-oxo-1,6-dihvdropyridazin-3-yl)methyl)phenyl)tetrahydro-2H-pyran-3,4.5-triyI triacetate

Chemical Property of (2R,3R,4R,5S,6S)-2-(acetoxymethyl)-6-(4-chIoro-3-((5-methyl-6-oxo-1,6-dihvdropyridazin-3-yl)methyl)phenyl)tetrahydro-2H-pyran-3,4.5-triyI triacetate

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Technology Process of (2R,3R,4R,5S,6S)-2-(acetoxymethyl)-6-(4-chIoro-3-((5-methyl-6-oxo-1,6-dihvdropyridazin-3-yl)methyl)phenyl)tetrahydro-2H-pyran-3,4.5-triyI triacetate

There total 1 articles about (2R,3R,4R,5S,6S)-2-(acetoxymethyl)-6-(4-chIoro-3-((5-methyl-6-oxo-1,6-dihvdropyridazin-3-yl)methyl)phenyl)tetrahydro-2H-pyran-3,4.5-triyI triacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

6-(2-chloro-5-((2S,3R,4R,5S,6R)-3,4,5-trihydroxy-6-(hydroxymethyl)tetrahydro-2H-pyran-yl)benzyl)-4-methylpyridazin-3(2H)-one (1259019-56-1) + acetic anhydride (108-24-7) → (2R,3R,4R,5S,6S)-2-(acetoxymethyl)-6-(4-chIoro-3-((5-methyl-6-oxo-1,6-dihvdropyridazin-3-yl)methyl)phenyl)tetrahydro-2H-pyran-3,4.5-triyI triacetate (1259019-52-7)

Guidance literature:

With dmap; triethylamine; In dichloromethane; for 5h; Inert atmosphere;

Reference yield: 70.0%

(2R,3R,4R,5S,6S)-2-(acetoxymethyl)-6-(4-chIoro-3-((5-methyl-6-oxo-1,6-dihvdropyridazin-3-yl)methyl)phenyl)tetrahydro-2H-pyran-3,4.5-triyI triacetate (1259019-52-7) → (2R,3R,4R,5S,6S)-2-(acetoxymethyl)-6-(4-chIoro-3-((6-chloro-5-methylpyridazin-3-yl)methyl)phenyl)tetrahydro-2H-pyran-3,4.5-triyI triacetate (1259019-54-9)

Guidance literature:

With trichlorophosphate; In toluene; at 20 - 70 ℃;

upstream raw materials:

6-(2-chloro-5-((2S,3R,4R,5S,6R)-3,4,5-trihydroxy-6-(hydroxymethyl)tetrahydro-2H-pyran-yl)benzyl)-4-methylpyridazin-3(2H)-one

acetic anhydride

Downstream raw materials:

(2R,3R,4R,5S,6S)-2-(acetoxymethyl)-6-(4-chIoro-3-((6-chloro-5-methylpyridazin-3-yl)methyl)phenyl)tetrahydro-2H-pyran-3,4.5-triyI triacetate

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