5-(4-cyclobutyl-2-phenylsulfonyl-2,3-butadienyl)-2,2-dimethyl-5-(2-propynyl)-1,3-dioxane

Base Information

Chemical Name:5-(4-cyclobutyl-2-phenylsulfonyl-2,3-butadienyl)-2,2-dimethyl-5-(2-propynyl)-1,3-dioxane
CAS No.:1333467-06-3
Molecular Formula:C₂₃H₂₈O₄S
Molecular Weight:400.539
Hs Code.:

Synonyms:5-(4-cyclobutyl-2-phenylsulfonyl-2,3-butadienyl)-2,2-dimethyl-5-(2-propynyl)-1,3-dioxane

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Chemical Property of 5-(4-cyclobutyl-2-phenylsulfonyl-2,3-butadienyl)-2,2-dimethyl-5-(2-propynyl)-1,3-dioxane

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Technology Process of 5-(4-cyclobutyl-2-phenylsulfonyl-2,3-butadienyl)-2,2-dimethyl-5-(2-propynyl)-1,3-dioxane

There total 4 articles about 5-(4-cyclobutyl-2-phenylsulfonyl-2,3-butadienyl)-2,2-dimethyl-5-(2-propynyl)-1,3-dioxane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₃H₂₈O₃S

: 1333467-06-3
5-(4-cyclobutyl-2-phenylsulfonyl-2,3-butadienyl)-2,2-dimethyl-5-(2-propynyl)-1,3-dioxane

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 0 ℃; for 0.5h; Inert atmosphere;
DOI:10.1002/chem.201101441

Reference yield:

: 1333467-22-3
5-(4-cyclobutyl-4-hydroxy-2-butynyl)-2,2-dimethyl-5-(2-propynyl)-1,3-dioxane

: 1333467-06-3
5-(4-cyclobutyl-2-phenylsulfonyl-2,3-butadienyl)-2,2-dimethyl-5-(2-propynyl)-1,3-dioxane

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / tetrahydrofuran / -78 °C / Inert atmosphere

2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

With triethylamine; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; dichloromethane;
DOI:10.1002/chem.201101441

Reference yield:

: 2987-17-9
cyclobutylaldehyde

: 1333467-06-3
5-(4-cyclobutyl-2-phenylsulfonyl-2,3-butadienyl)-2,2-dimethyl-5-(2-propynyl)-1,3-dioxane

Guidance literature:: Multi-step reaction with 3 steps

1.1: lithium hexamethyldisilazane / tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

1.2: 0.08 h / -78 °C / Inert atmosphere

2.1: triethylamine / tetrahydrofuran / -78 °C / Inert atmosphere

3.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

With triethylamine; 3-chloro-benzenecarboperoxoic acid; lithium hexamethyldisilazane; In tetrahydrofuran; dichloromethane;
DOI:10.1002/chem.201101441