benzyl 3-O-benzyl-2-O-(2,3,4-tri-O-benzyl-α-L-rhamnopyranosyl)-β-L-arabinopyranoside

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Chemical Name:benzyl 3-O-benzyl-2-O-(2,3,4-tri-O-benzyl-α-L-rhamnopyranosyl)-β-L-arabinopyranoside
CAS No.:86049-13-0
Molecular Formula:C₄₆H₅₀O₉
Molecular Weight:746.898
Hs Code.:

Synonyms:benzyl 3-O-benzyl-2-O-(2,3,4-tri-O-benzyl-α-L-rhamnopyranosyl)-β-L-arabinopyranoside

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Chemical Property of benzyl 3-O-benzyl-2-O-(2,3,4-tri-O-benzyl-α-L-rhamnopyranosyl)-β-L-arabinopyranoside

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Technology Process of benzyl 3-O-benzyl-2-O-(2,3,4-tri-O-benzyl-α-L-rhamnopyranosyl)-β-L-arabinopyranoside

There total 5 articles about benzyl 3-O-benzyl-2-O-(2,3,4-tri-O-benzyl-α-L-rhamnopyranosyl)-β-L-arabinopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.8%

: 86049-07-2,86117-04-6
benzyl exo-3,4-O-benzylidene-2-O-(2,3,4-tri-O-benzyl-α-L-rhamnopyranosyl)-β-L-arabinopyranoside

: 86049-13-0
benzyl 3-O-benzyl-2-O-(2,3,4-tri-O-benzyl-α-L-rhamnopyranosyl)-β-L-arabinopyranoside

: 86049-12-9
benzyl 4-O-benzyl-2-O-(2,3,4-tri-O-benzyl-α-L-rhamnopyranosyl)-β-L-arabinopyranoside

Guidance literature:: With lithium aluminium tetrahydride; aluminium trichloride; In diethyl ether; dichloromethane; for 0.25h; Heating;
DOI:10.1016/0040-4020(82)85034-5

Reference yield:

: 39524-38-4
2,3,4-tri-O-acetyl-6-deoxy-beta-L-mannopyranosyl bromide

: 86049-13-0
benzyl 3-O-benzyl-2-O-(2,3,4-tri-O-benzyl-α-L-rhamnopyranosyl)-β-L-arabinopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: Hg(CN)2 / benzene; nitromethane / 1 h / 45 °C

2: 1) 1N NaOMe; 2) KOH / 1) MeOH, room temp., 16 h; 2) 100 deg C, 4 h

3: 22.4 percent / LiAlH₄, AlCl₃ / CH₂Cl₂; diethyl ether / 0.25 h / Heating

With potassium hydroxide; lithium aluminium tetrahydride; aluminium trichloride; sodium methylate; mercury(II) cyanide; In diethyl ether; nitromethane; dichloromethane; benzene;
DOI:10.1016/0040-4020(82)85034-5

Reference yield:

: 79936-13-3
benzyl exo-3,4-O-benzylidene-β-L-arabinopyranoside

: 86049-13-0
benzyl 3-O-benzyl-2-O-(2,3,4-tri-O-benzyl-α-L-rhamnopyranosyl)-β-L-arabinopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 71 percent / Hg(CN)2 / benzene; nitromethane / 0.75 h / 45 °C

2: 1) 1N NaOMe; 2) KOH / 1) MeOH, room temp., 16 h; 2) 100 deg C, 4 h

3: 22.4 percent / LiAlH₄, AlCl₃ / CH₂Cl₂; diethyl ether / 0.25 h / Heating

With potassium hydroxide; lithium aluminium tetrahydride; aluminium trichloride; sodium methylate; mercury(II) cyanide; In diethyl ether; nitromethane; dichloromethane; benzene;
DOI:10.1016/0040-4020(82)85034-5