Technology Process of C17H21F3O6S
There total 9 articles about C17H21F3O6S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
pyridine;
In
dichloromethane;
at 0 - 20 ℃;
for 0.25 - 0.5h;
Product distribution / selectivity;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: lithium diisopropyl amide / tetrahydrofuran; tris(pyrrolidino)phosphine oxide / -60 °C
2.1: hydrogen / palladium 10% on activated carbon / methanol / 2250.23 Torr
3.1: di(n-butyl)tin oxide / toluene / 4 h / Heating / reflux
3.2: 22 h / 90 °C
4.1: pyridine / dichloromethane / 0.25 - 0.5 h / 0 - 20 °C
With
pyridine; hydrogen; di(n-butyl)tin oxide; lithium diisopropyl amide;
palladium 10% on activated carbon;
In
tetrahydrofuran; methanol; dichloromethane; tris(pyrrolidino)phosphine oxide; toluene;
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: tetrahydrofuran / 2 h / Heating / reflux
2.1: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride / toluene / 0.33 h / 100 °C
3.1: boron trifluoride diethyl etherate; 3-chloro-benzenecarboperoxoic acid / dichloromethane / 17 h / 0 - 20 °C
4.1: lithium diisopropyl amide / tetrahydrofuran; tris(pyrrolidino)phosphine oxide / -60 °C
5.1: hydrogen / palladium 10% on activated carbon / methanol / 2250.23 Torr
6.1: di(n-butyl)tin oxide / toluene / 4 h / Heating / reflux
6.2: 22 h / 90 °C
7.1: pyridine / dichloromethane / 0.25 - 0.5 h / 0 - 20 °C
With
pyridine; 2,2'-azobis(isobutyronitrile); boron trifluoride diethyl etherate; hydrogen; tri-n-butyl-tin hydride; di(n-butyl)tin oxide; 3-chloro-benzenecarboperoxoic acid; lithium diisopropyl amide;
palladium 10% on activated carbon;
In
tetrahydrofuran; methanol; dichloromethane; tris(pyrrolidino)phosphine oxide; toluene;