Methyl-16-hydroxy-cis-9-hexadecenoat

Base Information

Chemical Name:Methyl-16-hydroxy-cis-9-hexadecenoat
CAS No.:53837-83-5
Molecular Formula:C₁₇H₃₂O₃
Molecular Weight:284.439
Hs Code.:

Synonyms:Methyl-16-hydroxy-cis-9-hexadecenoat

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Chemical Property of Methyl-16-hydroxy-cis-9-hexadecenoat

Chemical Property:

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Technology Process of Methyl-16-hydroxy-cis-9-hexadecenoat

There total 1 articles about Methyl-16-hydroxy-cis-9-hexadecenoat which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 25601-41-6
methyl 9-decenoate

: 20731-23-1
methyl non-8-enoate

: 53837-83-5
Methyl-16-hydroxy-cis-9-hexadecenoat

: 78924-81-9
methyl 16-hydroxy-(E)-9-hexadecenoate

Guidance literature:: methyl 9-decenoate; methyl non-8-enoate; With N-{[(1-{2-[(tert-butyldimethylsilyl)oxy]-3-(trifluoromethyl)-5,6,7,8-tetrahydronaphthalen-1-yl}-3-(trifluoromethyl)-5,6,7,8-tetrahydronaphthalen-2-yl)oxy](2,5-dimethyl-1H-pyrrol-1-yl)(2-methyl-2-phenylpropylidene)molybdenumylidene}adamantan-1-amine; In benzene; at 20 ℃; for 6h; Inert atmosphere; Glovebox;

With sodium methylate; In methanol; at 20 ℃; for 2h; Overall yield = 68 %; Overall yield = 355 mg;

Reference yield:

: 53837-83-5
Methyl-16-hydroxy-cis-9-hexadecenoat

: 2536-34-7
16-chlorohexadecanoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: PPh₃, CCl₄ / Heating

2: aq. NaOH

3: H₂ / Pd/C / Ambient temperature

With tetrachloromethane; sodium hydroxide; hydrogen; triphenylphosphine; palladium on activated charcoal;

Reference yield:

: 53837-83-5
Methyl-16-hydroxy-cis-9-hexadecenoat

: 2,5-dioxopyrrolidin-1-yl (Z)-15-(4,5-dimethoxy-2-methyl-3,6-dioxocyclohexa-1,4-dien-1-yl)pentadec-9-enoate

Guidance literature:: Multi-step reaction with 4 steps

1: chromium(VI) oxide; acetic acid / acetone / 2 h / 0 - 25 °C

2: silver nitrate; dipotassium peroxodisulfate / acetonitrile; water / 2 h / 25 - 75 °C

3: hydrogenchloride / 1,4-dioxane / 18 h / 0 - 40 °C

4: 1-hydroxy-pyrrolidine-2,5-dione; dicyclohexyl-carbodiimide / ethyl acetate / 18 h / 25 °C

With chromium(VI) oxide; hydrogenchloride; dipotassium peroxodisulfate; 1-hydroxy-pyrrolidine-2,5-dione; silver nitrate; acetic acid; dicyclohexyl-carbodiimide; In 1,4-dioxane; water; ethyl acetate; acetone; acetonitrile;