2,2-difluoro-1-O-allyl-3,6-di-O-benzyl-4,5-O-isopropylidene myo-inositol

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Chemical Name:2,2-difluoro-1-O-allyl-3,6-di-O-benzyl-4,5-O-isopropylidene myo-inositol
CAS No.:127414-72-6
Molecular Formula:C₂₆H₃₀F₂O₅
Molecular Weight:460.518
Hs Code.:

Synonyms:2,2-difluoro-1-O-allyl-3,6-di-O-benzyl-4,5-O-isopropylidene myo-inositol

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Chemical Property of 2,2-difluoro-1-O-allyl-3,6-di-O-benzyl-4,5-O-isopropylidene myo-inositol

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Technology Process of 2,2-difluoro-1-O-allyl-3,6-di-O-benzyl-4,5-O-isopropylidene myo-inositol

There total 4 articles about 2,2-difluoro-1-O-allyl-3,6-di-O-benzyl-4,5-O-isopropylidene myo-inositol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 114218-27-8
(+/-)-1-O-allyl-3,6-di-O-benzyl-4,5-O-isopropylidene-myo-inosose-2

: 127414-72-6
(+/-)-1-O-allyl-3,6-di-O-benzyl-2-deoxy-2,2-difluoro-4,5-O-isopropylidene-myo-inositol

Guidance literature:: With diethylamino-sulfur trifluoride; In dichloromethane; for 5h; Ambient temperature;

Reference yield: 60.0%

: 114218-27-8
(3aS,4R,6S,7R,7aR)-6-Allyloxy-4,7-bis-benzyloxy-2,2-dimethyl-tetrahydro-benzo[1,3]dioxol-5-one

: 127414-72-6
2,2-difluoro-1-O-allyl-3,6-di-O-benzyl-4,5-O-isopropylidene myo-inositol

Guidance literature:: With 4,4'-diaminostilbene-2,2'-disulfonic acid; In dichloromethane; at 25 ℃;
DOI:10.1016/S0040-4039(01)80578-5

Reference yield:

: 114218-23-4,114297-87-9,114298-50-9
1-O-allyl-3,6-di-O-benzyl-4,5-O-isopropylidene-myo-inositol

: 127414-72-6
2,2-difluoro-1-O-allyl-3,6-di-O-benzyl-4,5-O-isopropylidene myo-inositol

Guidance literature:: Multi-step reaction with 2 steps

1: 66 percent / acetic anhydride / dimethylsulfoxide

2: 60 percent / DAST / CH₂Cl₂ / 25 °C

With acetic anhydride; 4,4'-diaminostilbene-2,2'-disulfonic acid; In dichloromethane; dimethyl sulfoxide;
DOI:10.1016/S0040-4039(01)80578-5