Acetic acid (2S,3R,4S,5R,6R)-4,5-diacetoxy-6-acetoxymethyl-2-(3-cyano-6-phenyl-4-thiophen-2-yl-pyridin-2-ylsulfanyl)-tetrahydro-pyran-3-yl ester

Base Information

• Chemical Name: Acetic acid (2S,3R,4S,5R,6R)-4,5-diacetoxy-6-acetoxymethyl-2-(3-cyano-6-phenyl-4-thiophen-2-yl-pyridin-2-ylsulfanyl)-tetrahydro-pyran-3-yl ester
• CAS No.: 618386-72-4
• Molecular Formula: C₃₀H₂₈N₂O₉S₂
• Molecular Weight: 624.692

Synonyms:Acetic acid (2S,3R,4S,5R,6R)-4,5-diacetoxy-6-acetoxymethyl-2-(3-cyano-6-phenyl-4-thiophen-2-yl-pyridin-2-ylsulfanyl)-tetrahydro-pyran-3-yl ester

Chemical Property of Acetic acid (2S,3R,4S,5R,6R)-4,5-diacetoxy-6-acetoxymethyl-2-(3-cyano-6-phenyl-4-thiophen-2-yl-pyridin-2-ylsulfanyl)-tetrahydro-pyran-3-yl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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Technology Process of Acetic acid (2S,3R,4S,5R,6R)-4,5-diacetoxy-6-acetoxymethyl-2-(3-cyano-6-phenyl-4-thiophen-2-yl-pyridin-2-ylsulfanyl)-tetrahydro-pyran-3-yl ester

There total 6 articles about Acetic acid (2S,3R,4S,5R,6R)-4,5-diacetoxy-6-acetoxymethyl-2-(3-cyano-6-phenyl-4-thiophen-2-yl-pyridin-2-ylsulfanyl)-tetrahydro-pyran-3-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(E)-1-phenyl-3-(thiophen-2-yl)-2-propen-1-one (39511-11-0) + Acetic acid (2R,3R,4S,5R,6S)-3,5-diacetoxy-2-acetoxymethyl-6-(2-cyano-acetimidoylsulfanyl)-tetrahydro-pyran-4-yl ester (618386-55-3) → Acetic acid (2S,3R,4S,5R,6R)-4,5-diacetoxy-6-acetoxymethyl-2-(3-cyano-6-phenyl-4-thiophen-2-yl-pyridin-2-ylsulfanyl)-tetrahydro-pyran-3-yl ester (618386-72-4)

Guidance literature:

With piperidine; In ethanol; at 60 ℃;

DOI:10.1081/SCC-120021503

Reference yield:

6-phenyl-4-thiophen-2-yl-2-trimethylsilanylsulfanyl-nicotinonitrile (618386-69-9) + β-D-glucose pentaacetate (604-69-3) → Acetic acid (2S,3R,4S,5R,6R)-4,5-diacetoxy-6-acetoxymethyl-2-(3-cyano-6-phenyl-4-thiophen-2-yl-pyridin-2-ylsulfanyl)-tetrahydro-pyran-3-yl ester (618386-72-4)

Guidance literature:

With tin(IV) chloride; In acetonitrile; at 0 ℃;

DOI:10.1081/SCC-120021503

Reference yield:

Acetic acid (2S,3R,4S,5R,6R)-4,5-diacetoxy-6-acetoxymethyl-2-(3-cyano-6-phenyl-4-thiophen-2-yl-1,4-dihydro-pyridin-2-ylsulfanyl)-tetrahydro-pyran-3-yl ester (618386-59-7) → Acetic acid (2S,3R,4S,5R,6R)-4,5-diacetoxy-6-acetoxymethyl-2-(3-cyano-6-phenyl-4-thiophen-2-yl-pyridin-2-ylsulfanyl)-tetrahydro-pyran-3-yl ester (618386-72-4)

Guidance literature:

With air; In ethanol; for 0.05h; Heating;

DOI:10.1081/SCC-120021503

upstream raw materials:

(E)-1-phenyl-3-(thiophen-2-yl)-2-propen-1-one

Acetic acid (2R,3R,4S,5R,6S)-3,5-diacetoxy-2-acetoxymethyl-6-(2-cyano-acetimidoylsulfanyl)-tetrahydro-pyran-4-yl ester

Acetic acid (2S,3R,4S,5R,6R)-4,5-diacetoxy-6-acetoxymethyl-2-(3-cyano-6-phenyl-4-thiophen-2-yl-1,4-dihydro-pyridin-2-ylsulfanyl)-tetrahydro-pyran-3-yl ester

2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl bromide

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