[(1S,2R)-1-((R)-2-Benzyloxy-1-methyl-ethyl)-2-methyl-but-3-enyloxy]-tert-butyl-dimethyl-silane

Base Information

Chemical Name:[(1S,2R)-1-((R)-2-Benzyloxy-1-methyl-ethyl)-2-methyl-but-3-enyloxy]-tert-butyl-dimethyl-silane
CAS No.:443283-58-7
Molecular Formula:C₂₁H₃₆O₂Si
Molecular Weight:348.601
Hs Code.:

Synonyms:[(1S,2R)-1-((R)-2-Benzyloxy-1-methyl-ethyl)-2-methyl-but-3-enyloxy]-tert-butyl-dimethyl-silane

Suppliers and Price of [(1S,2R)-1-((R)-2-Benzyloxy-1-methyl-ethyl)-2-methyl-but-3-enyloxy]-tert-butyl-dimethyl-silane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [(1S,2R)-1-((R)-2-Benzyloxy-1-methyl-ethyl)-2-methyl-but-3-enyloxy]-tert-butyl-dimethyl-silane

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of [(1S,2R)-1-((R)-2-Benzyloxy-1-methyl-ethyl)-2-methyl-but-3-enyloxy]-tert-butyl-dimethyl-silane

There total 2 articles about [(1S,2R)-1-((R)-2-Benzyloxy-1-methyl-ethyl)-2-methyl-but-3-enyloxy]-tert-butyl-dimethyl-silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 69739-34-0
t-butyldimethylsiyl triflate

: 119065-12-2
(3R,4S,5R)-6-(benzyloxy)-3,5-dimethyl-1-hexen-4-ol

: 443283-58-7
[(1S,2R)-1-((R)-2-Benzyloxy-1-methyl-ethyl)-2-methyl-but-3-enyloxy]-tert-butyl-dimethyl-silane

Guidance literature:: With 2,6-dimethylpyridine; In dichloromethane; for 0.5h;
DOI:10.1021/jo016413f

Reference yield:

: 79026-61-2
(R)-3-benzyloxy-2-methylpropanal

: 443283-58-7
[(1S,2R)-1-((R)-2-Benzyloxy-1-methyl-ethyl)-2-methyl-but-3-enyloxy]-tert-butyl-dimethyl-silane

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / TiCl₄ / 2.5 h / -90 °C

2: 83 percent / Et₃N / CH₂Cl₂ / 1 h / -30 - 0 °C

With titanium tetrachloride; triethylamine; In dichloromethane;
DOI:10.1016/j.tetlet.2005.04.146

Reference yield: 83.0%

: 443283-58-7
[(1S,2R)-1-((R)-2-Benzyloxy-1-methyl-ethyl)-2-methyl-but-3-enyloxy]-tert-butyl-dimethyl-silane

: 143245-42-5
6-benzyloxy-4-[(tert-butyldimethylsiltl)oxy]-3,5-dimethylhexan-2-one

Guidance literature:: With oxygen; copper(l) chloride; palladium dichloride; In water; N,N-dimethyl-formamide; at 23 ℃; for 72h;
DOI:10.1021/jo016413f