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C27H40O9

Base Information
  • Chemical Name:C27H40O9
  • CAS No.:1449216-20-9
  • Molecular Formula:C27H40O9
  • Molecular Weight:508.609
  • Hs Code.:
C<sub>27</sub>H<sub>40</sub>O<sub>9</sub>

Synonyms:C27H40O9

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Chemical Property of C27H40O9
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Technology Process of C27H40O9

There total 10 articles about C27H40O9 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With pyridine; pyridine hydrogenfluoride; In tetrahydrofuran; at 4 ℃; for 11.5h;
DOI:10.3987/COM-12-S(N)8
Guidance literature:
Multi-step reaction with 7 steps
1.1: 4-methylmorpholine N-oxide; tetrapropylammonium perruthennate / dichloromethane / 0.5 h / 20 °C / Molecular sieve
2.1: silver(l) oxide; titanium tetrachloride; titanium(IV) isopropylate; (S)-[1,1']-binaphthalenyl-2,2'-diol / dichloromethane; diethyl ether / 21 h / -15 - 4 °C / Inert atmosphere
3.1: acetic acid / tetrahydrofuran; water / 0.83 h / 55 °C
4.1: mercury(II) perchlorate hexahydrate / dichloromethane; water; acetonitrile / 0.75 h / 4 °C
5.1: triethylamine; 2,4,6-trichlorobenzoyl chloride / toluene / 2 h / 20 °C
5.2: 1.5 h / 20 - 50 °C
6.1: sodium periodate; potassium permanganate / tert-butyl alcohol / 1 h / 20 °C / pH 7.2
7.1: pyridine hydrogenfluoride; pyridine / tetrahydrofuran / 11.5 h / 4 °C
With pyridine; titanium(IV) isopropylate; potassium permanganate; sodium periodate; tetrapropylammonium perruthennate; mercury(II) perchlorate hexahydrate; 2,4,6-trichlorobenzoyl chloride; (S)-[1,1']-binaphthalenyl-2,2'-diol; titanium tetrachloride; pyridine hydrogenfluoride; acetic acid; 4-methylmorpholine N-oxide; triethylamine; silver(l) oxide; In tetrahydrofuran; diethyl ether; dichloromethane; water; toluene; acetonitrile; tert-butyl alcohol; 1.1: |Ley Oxidation;
DOI:10.3987/COM-12-S(N)8
Guidance literature:
Multi-step reaction with 6 steps
1.1: silver(l) oxide; titanium tetrachloride; titanium(IV) isopropylate; (S)-[1,1']-binaphthalenyl-2,2'-diol / dichloromethane; diethyl ether / 21 h / -15 - 4 °C / Inert atmosphere
2.1: acetic acid / tetrahydrofuran; water / 0.83 h / 55 °C
3.1: mercury(II) perchlorate hexahydrate / dichloromethane; water; acetonitrile / 0.75 h / 4 °C
4.1: triethylamine; 2,4,6-trichlorobenzoyl chloride / toluene / 2 h / 20 °C
4.2: 1.5 h / 20 - 50 °C
5.1: sodium periodate; potassium permanganate / tert-butyl alcohol / 1 h / 20 °C / pH 7.2
6.1: pyridine hydrogenfluoride; pyridine / tetrahydrofuran / 11.5 h / 4 °C
With pyridine; titanium(IV) isopropylate; potassium permanganate; sodium periodate; mercury(II) perchlorate hexahydrate; 2,4,6-trichlorobenzoyl chloride; (S)-[1,1']-binaphthalenyl-2,2'-diol; titanium tetrachloride; pyridine hydrogenfluoride; acetic acid; triethylamine; silver(l) oxide; In tetrahydrofuran; diethyl ether; dichloromethane; water; toluene; acetonitrile; tert-butyl alcohol;
DOI:10.3987/COM-12-S(N)8
upstream raw materials:

C36H56O4S2Si

C39H60O4S2Si

C17H28O4Si

Downstream raw materials:

C27H36O8

C41H48O8

C41H48O8

C48H54O9

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