6-amine-6-deoxy-1,2-O-isopropylidene-3-C-methyl-3-O-benzyl-α-allofuranose

Base Information

Chemical Name:6-amine-6-deoxy-1,2-O-isopropylidene-3-C-methyl-3-O-benzyl-α-allofuranose
CAS No.:1350745-09-3
Molecular Formula:C₁₇H₂₅NO₅
Molecular Weight:323.389
Hs Code.:

Synonyms:6-amine-6-deoxy-1,2-O-isopropylidene-3-C-methyl-3-O-benzyl-α-allofuranose

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Chemical Property of 6-amine-6-deoxy-1,2-O-isopropylidene-3-C-methyl-3-O-benzyl-α-allofuranose

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Technology Process of 6-amine-6-deoxy-1,2-O-isopropylidene-3-C-methyl-3-O-benzyl-α-allofuranose

There total 2 articles about 6-amine-6-deoxy-1,2-O-isopropylidene-3-C-methyl-3-O-benzyl-α-allofuranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1350745-12-8
6-azido-6-deoxy-1,2-O-isopropylidene-3-C-methyl-3-benzyl-α-allofuranose

: 1350745-09-3
6-amine-6-deoxy-1,2-O-isopropylidene-3-C-methyl-3-O-benzyl-α-allofuranose

Guidance literature:: With water; triphenylphosphine; In tetrahydrofuran; at 20 ℃; Inert atmosphere;
DOI:10.1039/c1cc15024c

Reference yield:

: 99050-12-1
3-O-Benzyl-1,2-O-isopropyliden-3-C-methyl-6-O-(p-tolylsulfonyl)-α-D-allo-hexofuranose

: 1350745-09-3
6-amine-6-deoxy-1,2-O-isopropylidene-3-C-methyl-3-O-benzyl-α-allofuranose

Guidance literature:: Multi-step reaction with 2 steps

1: sodium azide / N,N-dimethyl-formamide / 90 °C / Inert atmosphere

2: water; triphenylphosphine / tetrahydrofuran / 20 °C / Inert atmosphere

With sodium azide; water; triphenylphosphine; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1039/c1cc15024c

Reference yield:

: 1350745-09-3
6-amine-6-deoxy-1,2-O-isopropylidene-3-C-methyl-3-O-benzyl-α-allofuranose

: 2900-27-8
(2S)-2-[(tert-butoxycarbonyl)amino]-2-phenylethanoic acid

: 1350745-03-7
C₃₀H₄₀N₂O₈

Guidance literature:: (2S)-2-[(tert-butoxycarbonyl)amino]-2-phenylethanoic acid; With 4-methyl-morpholine; isobutyl chloroformate; In tetrahydrofuran; at -15 ℃; for 0.75h; Inert atmosphere; Schlenk technique;

6-amine-6-deoxy-1,2-O-isopropylidene-3-C-methyl-3-O-benzyl-α-allofuranose; In tetrahydrofuran; at 20 ℃; for 2h; Inert atmosphere; Schlenk technique;
DOI:10.1002/cctc.201300456