Technology Process of C17H24FNO4S
There total 3 articles about C17H24FNO4S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
lanthanum(lll) triflate;
In
toluene;
at 20 ℃;
for 10h;
optical yield given as %de;
diastereoselective reaction;
Molecular sieve;
Inert atmosphere;
DOI:10.1021/ol301180z
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium periodate / water
2: copper(II) sulfate / dichloromethane / 48 h / 20 °C
3: lanthanum(lll) triflate / toluene / 10 h / 20 °C / Molecular sieve; Inert atmosphere
With
sodium periodate; copper(II) sulfate; lanthanum(lll) triflate;
In
dichloromethane; water; toluene;
3: Mannich reaction;
DOI:10.1021/ol301180z
- Guidance literature:
-
Multi-step reaction with 2 steps
1: copper(II) sulfate / dichloromethane / 48 h / 20 °C
2: lanthanum(lll) triflate / toluene / 10 h / 20 °C / Molecular sieve; Inert atmosphere
With
copper(II) sulfate; lanthanum(lll) triflate;
In
dichloromethane; toluene;
2: Mannich reaction;
DOI:10.1021/ol301180z