(^Me(Ph)PDI)FeCl₂

Base Information

Chemical Name:(^Me(Ph)PDI)FeCl₂
CAS No.:301658-90-2
Molecular Formula:C₃₅H₃₁Cl₂FeN₃
Molecular Weight:620.404
Hs Code.:

Synonyms:(^Me(Ph)PDI)FeCl₂

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Chemical Property of (^Me(Ph)PDI)FeCl₂

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Technology Process of (^Me(Ph)PDI)FeCl₂

There total 1 articles about (^Me(Ph)PDI)FeCl₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: iron(II) chloride

: 301658-89-9
2,6-bis(1-[(2,6-dimethylphenyl)imino]-benzyl)pyridine

: 301658-90-2
(^Me(Ph)PDI)FeCl₂

Guidance literature:: In tetrahydrofuran; diethyl ether; (Ar), mixed (1:1 solvent mixture), stirred at room temp. for 10 h; filtered, washed (diethyl ether), dried, MAS;
DOI:10.1016/S1381-1169(01)00333-8

Reference yield: 63.0%

: 301658-90-2
(^Me(Ph)PDI)FeCl₂

: 106-99-0,130983-70-9,29406-96-0,9003-17-2
buta-1,3-diene

: (^Me(Ph)PDI)Fe(s-trans C₄H₆)

Guidance literature:: With sodium; mercury; In toluene; at 20 ℃; for 24h; Schlenk technique; Glovebox; Inert atmosphere;
DOI:10.1021/jacs.1c08912

Reference yield: 45.0%

: 109-99-9,24979-97-3,77392-70-2
tetrahydrofuran

: 301658-90-2
(^Me(Ph)PDI)FeCl₂

: 7727-37-9
nitrogen

: 1214787-06-0
(2,6-(2,6-Me₂C₆H₃N=CPh)2C₅H₃N)Fe(THF)2

: 1214787-03-7
[(2,6-(2,6-Me2C6H3N=CPh)2C5H3N)Fe(N2)]2(μ2-N2)

Guidance literature:: With Na; naphthalene; In tetrahydrofuran; byproducts: NaBr; (N2); addn. of THF to a mixt. of iron complex, Na (2 equivs.), naphthalene (0.05 equiv.), stirring for 1.5 h; evapn. in vac., addn. of Et2O, filtration through Celite, evapn. in vac., recrystn. (Et2O, -35°C);
DOI:10.1021/ic902162z