(5R)-benzyl 2,3-O-isopropylidene-4-O-methyl-5-C-(1H-tetrazol-5-yl)-α-D-lyxopyranoside

Base Information

Chemical Name:(5R)-benzyl 2,3-O-isopropylidene-4-O-methyl-5-C-(1H-tetrazol-5-yl)-α-D-lyxopyranoside
CAS No.:1382060-10-7
Molecular Formula:C₁₇H₂₂N₄O₅
Molecular Weight:362.385
Hs Code.:

Synonyms:(5R)-benzyl 2,3-O-isopropylidene-4-O-methyl-5-C-(1H-tetrazol-5-yl)-α-D-lyxopyranoside

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Chemical Property of (5R)-benzyl 2,3-O-isopropylidene-4-O-methyl-5-C-(1H-tetrazol-5-yl)-α-D-lyxopyranoside

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Technology Process of (5R)-benzyl 2,3-O-isopropylidene-4-O-methyl-5-C-(1H-tetrazol-5-yl)-α-D-lyxopyranoside

There total 7 articles about (5R)-benzyl 2,3-O-isopropylidene-4-O-methyl-5-C-(1H-tetrazol-5-yl)-α-D-lyxopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1382060-09-4
benzyl 2,3-O-isopropylidene-4-O-methyl-α-D-mannopyranosidurononitrile

: 1382060-10-7
(5R)-benzyl 2,3-O-isopropylidene-4-O-methyl-5-C-(1H-tetrazol-5-yl)-α-D-lyxopyranoside

Guidance literature:: With trimethylsilylazide; di(n-butyl)tin oxide; In toluene; at 120 ℃; for 16h;
DOI:10.1021/ol3013638

Reference yield:

: benzyl (6S)-3-O-methyl-4,5-O-isopropylidene-α-D-mannodialdo-6,2-pyranoside

: 1382060-10-7
(5R)-benzyl 2,3-O-isopropylidene-4-O-methyl-5-C-(1H-tetrazol-5-yl)-α-D-lyxopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine; hydroxylamine hydrochloride / methanol; water / 2 h / 20 °C

2: pyridine; methanesulfonyl chloride / 2 h / 0 - 20 °C / Inert atmosphere

3: trimethylsilylazide; di(n-butyl)tin oxide / toluene / 16 h / 120 °C

With pyridine; trimethylsilylazide; hydroxylamine hydrochloride; di(n-butyl)tin oxide; methanesulfonyl chloride; In methanol; water; toluene;
DOI:10.1021/ol3013638

Reference yield:

: C₁₇H₂₃NO₆

: 1382060-10-7
(5R)-benzyl 2,3-O-isopropylidene-4-O-methyl-5-C-(1H-tetrazol-5-yl)-α-D-lyxopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine; methanesulfonyl chloride / 2 h / 0 - 20 °C / Inert atmosphere

2: trimethylsilylazide; di(n-butyl)tin oxide / toluene / 16 h / 120 °C

With pyridine; trimethylsilylazide; di(n-butyl)tin oxide; methanesulfonyl chloride; In toluene;
DOI:10.1021/ol3013638