Technology Process of C24H32N2O4
There total 8 articles about C24H32N2O4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
tris-(dibenzylideneacetone)dipalladium(0); johnphos; sodium t-butanolate;
In
1,4-dioxane;
at 20 - 80 ℃;
for 17h;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: caesium carbonate / N,N-dimethyl-formamide / 80 °C
2: hydrogenchloride / 1,4-dioxane / 20 °C
3: sodium hydroxide; water
4: sodium t-butanolate; johnphos; tris-(dibenzylideneacetone)dipalladium(0) / 1,4-dioxane / 17 h / 20 - 80 °C / Inert atmosphere
With
hydrogenchloride; tris-(dibenzylideneacetone)dipalladium(0); water; caesium carbonate; sodium hydroxide; johnphos; sodium t-butanolate;
In
1,4-dioxane; N,N-dimethyl-formamide;
4: |Buchwald-Hartwig Coupling;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: dihydrogen peroxide; sodium hydroxide / water; tetrahydrofuran / 2 h / 0 °C
2: caesium carbonate / N,N-dimethyl-formamide / 80 °C
3: hydrogenchloride / 1,4-dioxane / 20 °C
4: sodium hydroxide; water
5: sodium t-butanolate; johnphos; tris-(dibenzylideneacetone)dipalladium(0) / 1,4-dioxane / 17 h / 20 - 80 °C / Inert atmosphere
With
hydrogenchloride; tris-(dibenzylideneacetone)dipalladium(0); water; dihydrogen peroxide; caesium carbonate; sodium hydroxide; johnphos; sodium t-butanolate;
In
tetrahydrofuran; 1,4-dioxane; water; N,N-dimethyl-formamide;
5: |Buchwald-Hartwig Coupling;