4-(5-(1-hydroxy-3,3,5-trimethylcyclohexyl)-4H-1,2,4-triazol-3-yl)phenol

Base Information

Chemical Name:4-(5-(1-hydroxy-3,3,5-trimethylcyclohexyl)-4H-1,2,4-triazol-3-yl)phenol
CAS No.:1373018-88-2
Molecular Formula:C₁₇H₂₃N₃O₂
Molecular Weight:301.389
Hs Code.:

Synonyms:4-(5-(1-hydroxy-3,3,5-trimethylcyclohexyl)-4H-1,2,4-triazol-3-yl)phenol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-(5-(1-hydroxy-3,3,5-trimethylcyclohexyl)-4H-1,2,4-triazol-3-yl)phenol

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Technology Process of 4-(5-(1-hydroxy-3,3,5-trimethylcyclohexyl)-4H-1,2,4-triazol-3-yl)phenol

There total 2 articles about 4-(5-(1-hydroxy-3,3,5-trimethylcyclohexyl)-4H-1,2,4-triazol-3-yl)phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.47%

: 40643-64-9
1-hydroxy-3,3,5-trimethyl-cyclohexanecarbonitrile

: 5351-23-5
4-hydroxybenzoic acid hydrazide

: 1373018-88-2
4-(5-(1-hydroxy-3,3,5-trimethylcyclohexyl)-4H-1,2,4-triazol-3-yl)phenol

Guidance literature:: With potassium carbonate; In butan-1-ol; at 115 ℃; Microwave irradiation;
DOI:10.1007/s00044-012-0043-9

Reference yield:

: 873-94-9
dihydroisophorone

: 1373018-88-2
4-(5-(1-hydroxy-3,3,5-trimethylcyclohexyl)-4H-1,2,4-triazol-3-yl)phenol

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydrogensulfite / water / 0.75 h / 40 - 50 °C

1.2: 1 h / 30 °C

2.1: potassium carbonate / butan-1-ol / 115 °C / Microwave irradiation

With potassium carbonate; sodium hydrogensulfite; In water; butan-1-ol;
DOI:10.1007/s00044-012-0043-9