Technology Process of C23H40O3Si
There total 3 articles about C23H40O3Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
trans-2-Butene;
With
n-butyllithium; potassium tert-butylate;
In
tetrahydrofuran;
at -78 - -50 ℃;
for 1h;
Inert atmosphere;
With
(+)-B-methoxydiisocamphenylborane;
In
tetrahydrofuran;
at -78 ℃;
for 0.5h;
Inert atmosphere;
C19H32O3Si;
With
boron trifluoride diethyl etherate;
In
tetrahydrofuran;
at -78 ℃;
for 5h;
Inert atmosphere;
DOI:10.1039/c2cc34187e
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: 2,6-dimethylpyridine / dichloromethane / 1 h / -78 °C / Inert atmosphere
2.1: 2,6-dimethylpyridine; sodium periodate; osmium(VIII) oxide / 1,4-dioxane; water; tert-butyl alcohol / 20 - 25 °C / Inert atmosphere
3.1: n-butyllithium; potassium tert-butylate / tetrahydrofuran / 1 h / -78 - -50 °C / Inert atmosphere
3.2: 0.5 h / -78 °C / Inert atmosphere
3.3: 5 h / -78 °C / Inert atmosphere
With
2,6-dimethylpyridine; sodium periodate; osmium(VIII) oxide; n-butyllithium; potassium tert-butylate;
In
tetrahydrofuran; 1,4-dioxane; dichloromethane; water; tert-butyl alcohol;
DOI:10.1039/c2cc34187e
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: 2,6-dimethylpyridine; sodium periodate; osmium(VIII) oxide / 1,4-dioxane; water; tert-butyl alcohol / 20 - 25 °C / Inert atmosphere
2.1: n-butyllithium; potassium tert-butylate / tetrahydrofuran / 1 h / -78 - -50 °C / Inert atmosphere
2.2: 0.5 h / -78 °C / Inert atmosphere
2.3: 5 h / -78 °C / Inert atmosphere
With
2,6-dimethylpyridine; sodium periodate; osmium(VIII) oxide; n-butyllithium; potassium tert-butylate;
In
tetrahydrofuran; 1,4-dioxane; water; tert-butyl alcohol;
DOI:10.1039/c2cc34187e
