sodium hydrogen (1-{[2-(4-chloro-2-methylphenoxy)acetyl]oxy}ethyl)phosphonate

Base Information

• Chemical Name: sodium hydrogen (1-{[2-(4-chloro-2-methylphenoxy)acetyl]oxy}ethyl)phosphonate
• CAS No.: 1097934-95-6
• Molecular Formula: C₁₁H₁₃ClO₆P*Na
• Molecular Weight: 330.637
• Mol file: 1097934-95-6.mol

Synonyms:sodium hydrogen (1-{[2-(4-chloro-2-methylphenoxy)acetyl]oxy}ethyl)phosphonate

Chemical Property of sodium hydrogen (1-{[2-(4-chloro-2-methylphenoxy)acetyl]oxy}ethyl)phosphonate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of sodium hydrogen (1-{[2-(4-chloro-2-methylphenoxy)acetyl]oxy}ethyl)phosphonate

There total 5 articles about sodium hydrogen (1-{[2-(4-chloro-2-methylphenoxy)acetyl]oxy}ethyl)phosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

C11H14ClO6P (1097934-45-6) → sodium hydrogen (1-{[2-(4-chloro-2-methylphenoxy)acetyl]oxy}ethyl)phosphonate (1097934-95-6)

Guidance literature:

With sodium hydroxide; In methanol; at 20 ℃; for 2h;

DOI:10.1080/10426507.2012.717147

Reference yield:

C17H30ClO6PSi2 → sodium hydrogen (1-{[2-(4-chloro-2-methylphenoxy)acetyl]oxy}ethyl)phosphonate (1097934-95-6)

Guidance literature:

Multi-step reaction with 2 steps

1: methanol / 30 °C

2: sodium hydroxide / methanol / 2 h / 20 °C

With methanol; sodium hydroxide; In methanol;

DOI:10.1080/10426507.2012.717147

Reference yield:

C13H18ClO6P → sodium hydrogen (1-{[2-(4-chloro-2-methylphenoxy)acetyl]oxy}ethyl)phosphonate (1097934-95-6)

Guidance literature:

Multi-step reaction with 3 steps

1: sodium iodide / acetonitrile / 2 h / 30 °C / Inert atmosphere; Darkness

2: methanol / 30 °C

3: sodium hydroxide / methanol / 2 h / 20 °C

With methanol; sodium iodide; sodium hydroxide; In methanol; acetonitrile;

DOI:10.1080/10426507.2012.717147

upstream raw materials:

C₁₁H₁₄ClO₆P

2-methyl-4-chlorophenoxyacetyl chloride

MCPA