bis-1,2-(diphenylphosphino)ethane(η-cycloheptatrienyl)hydridomolybdenum

Base Information

• Chemical Name: bis-1,2-(diphenylphosphino)ethane(η-cycloheptatrienyl)hydridomolybdenum
• CAS No.: 60767-22-8
• Molecular Formula: C₃₃H₃₂MoP₂
• Molecular Weight: 586.505

Synonyms:bis-1,2-(diphenylphosphino)ethane(η-cycloheptatrienyl)hydridomolybdenum

Chemical Property of bis-1,2-(diphenylphosphino)ethane(η-cycloheptatrienyl)hydridomolybdenum

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Technology Process of bis-1,2-(diphenylphosphino)ethane(η-cycloheptatrienyl)hydridomolybdenum

There total 1 articles about bis-1,2-(diphenylphosphino)ethane(η-cycloheptatrienyl)hydridomolybdenum which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

MoI(Ph2PCH2CH2PPh2)(η-cycloheptatrienyl) → bis-1,2-(diphenylphosphino)ethane(η-cycloheptatrienyl)hydridomolybdenum (60767-22-8)

Guidance literature:

With Na(AlH₂(OCH₂CH₂OMe)2; In toluene; benzene; reducing agent as a 70% soln. in benzene was added to a soln. of the complex in toluene under N2, the mixt. was heated to 90°C for 1.5 h; after cooling to room temp. water was added, org. phase separated and concd., petroleum ether was added, filtn., washing with cold petroleum ether;

DOI:10.1016/S0277-5387(00)84077-2

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