[9-(2-{2-[4-(2-amino-ethyl)-7,10-bis-ethoxycarbonylmethyl-1,4,7,10tetraaza-cyclododec-1-yl]-ethylcarbamoyl}-phenyl)-6-diethylamino-xanthen-3-ylidene]-diethyl-ammonium

Base Information

Chemical Name:[9-(2-{2-[4-(2-amino-ethyl)-7,10-bis-ethoxycarbonylmethyl-1,4,7,10tetraaza-cyclododec-1-yl]-ethylcarbamoyl}-phenyl)-6-diethylamino-xanthen-3-ylidene]-diethyl-ammonium
CAS No.:917865-71-5
Molecular Formula:C₄₈H₇₁N₈O₆
Molecular Weight:856.142
Hs Code.:

[9-(2-{2-[4-(2-amino-ethyl)-7,10-bis-ethoxycarbonylmethyl-1,4,7,10tetraaza-cyclododec-1-yl]-ethylcarbamoyl}-phenyl)-6-diethylamino-xanthen-3-ylidene]-diethyl-ammonium

Synonyms:[9-(2-{2-[4-(2-amino-ethyl)-7,10-bis-ethoxycarbonylmethyl-1,4,7,10tetraaza-cyclododec-1-yl]-ethylcarbamoyl}-phenyl)-6-diethylamino-xanthen-3-ylidene]-diethyl-ammonium

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Chemical Property of [9-(2-{2-[4-(2-amino-ethyl)-7,10-bis-ethoxycarbonylmethyl-1,4,7,10tetraaza-cyclododec-1-yl]-ethylcarbamoyl}-phenyl)-6-diethylamino-xanthen-3-ylidene]-diethyl-ammonium

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Technology Process of [9-(2-{2-[4-(2-amino-ethyl)-7,10-bis-ethoxycarbonylmethyl-1,4,7,10tetraaza-cyclododec-1-yl]-ethylcarbamoyl}-phenyl)-6-diethylamino-xanthen-3-ylidene]-diethyl-ammonium

There total 5 articles about [9-(2-{2-[4-(2-amino-ethyl)-7,10-bis-ethoxycarbonylmethyl-1,4,7,10tetraaza-cyclododec-1-yl]-ethylcarbamoyl}-phenyl)-6-diethylamino-xanthen-3-ylidene]-diethyl-ammonium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 917865-70-4
[9-(2-{2-[4-(2-tert-butoxycarbonylamino-ethyl)-7,10-bis-ethoxycarbonylmethyl-1,4,7,10tetraaza-cyclododec-1-yl]-ethylcarbamoyl}-phenyl)-6-diethylamino-xanthen-3-ylidene]-diethyl-ammonium

: 917865-71-5
[9-(2-{2-[4-(2-amino-ethyl)-7,10-bis-ethoxycarbonylmethyl-1,4,7,10tetraaza-cyclododec-1-yl]-ethylcarbamoyl}-phenyl)-6-diethylamino-xanthen-3-ylidene]-diethyl-ammonium

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 0.5h;
DOI:10.1039/b611442c

Reference yield:

: 917865-67-9
{9-[2-(2-bromo-ethylcarbamoyl)-phenyl]-6-diethylamino-xanthen-3-ylidene}-diethyl-ammonium

: 917865-71-5
[9-(2-{2-[4-(2-amino-ethyl)-7,10-bis-ethoxycarbonylmethyl-1,4,7,10tetraaza-cyclododec-1-yl]-ethylcarbamoyl}-phenyl)-6-diethylamino-xanthen-3-ylidene]-diethyl-ammonium

Guidance literature:: Multi-step reaction with 4 steps

1: 39 percent / triethylamine / ethanol / 24 h / Heating

2: 20 percent / triethylamine / CHCl₃ / 36 h / 20 °C

3: 83 percent / potassium carbonate; sodium iodide / acetonitrile / 24 h / Heating

4: 84 percent / TFA / CH₂Cl₂ / 0.5 h / 20 °C

With potassium carbonate; triethylamine; trifluoroacetic acid; sodium iodide; In ethanol; dichloromethane; chloroform; acetonitrile;
DOI:10.1039/b611442c

Reference yield:

: 917865-68-0
(6-diethylamino-9-{2-[2-(1,4,7,10tetraaza-cyclododec-1-yl)-ethylcarbamoyl]-phenyl}-xanthen-3-ylidene)-diethyl-ammonium

: 917865-71-5
[9-(2-{2-[4-(2-amino-ethyl)-7,10-bis-ethoxycarbonylmethyl-1,4,7,10tetraaza-cyclododec-1-yl]-ethylcarbamoyl}-phenyl)-6-diethylamino-xanthen-3-ylidene]-diethyl-ammonium

Guidance literature:: Multi-step reaction with 3 steps

1: 20 percent / triethylamine / CHCl₃ / 36 h / 20 °C

2: 83 percent / potassium carbonate; sodium iodide / acetonitrile / 24 h / Heating

3: 84 percent / TFA / CH₂Cl₂ / 0.5 h / 20 °C

With potassium carbonate; triethylamine; trifluoroacetic acid; sodium iodide; In dichloromethane; chloroform; acetonitrile;
DOI:10.1039/b611442c