(2R,2′R)-2,2′-((2-iodo-1,3-phenylene)bis(oxy))bis(N-mesitylpropanamide)

Base Information

Chemical Name:(2R,2′R)-2,2′-((2-iodo-1,3-phenylene)bis(oxy))bis(N-mesitylpropanamide)
CAS No.:1240403-17-1
Molecular Formula:C₃₁H₃₇IN₂O₄
Molecular Weight:628.55
Hs Code.:

Synonyms:(2R,2′R)-2,2′-((2-iodo-1,3-phenylene)bis(oxy))bis(N-mesitylpropanamide)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2R,2′R)-2,2′-((2-iodo-1,3-phenylene)bis(oxy))bis(N-mesitylpropanamide)

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Technology Process of (2R,2′R)-2,2′-((2-iodo-1,3-phenylene)bis(oxy))bis(N-mesitylpropanamide)

There total 6 articles about (2R,2′R)-2,2′-((2-iodo-1,3-phenylene)bis(oxy))bis(N-mesitylpropanamide) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: (2R,2′R)-2,2′-((2-iodo-5-methyl-1,3-phenylene)bis(oxy)dipropanoic acid)

: 88-05-1
2,4,6-trimethylaniline

: 1240403-17-1
(2R,2′R)-2,2′-((2-iodo-1,3-phenylene)bis(oxy))bis(N-mesitylpropanamide)

Guidance literature:: (2R,2′R)-2,2′-((2-iodo-5-methyl-1,3-phenylene)bis(oxy)dipropanoic acid); With oxalyl dichloride; In dichloromethane; at 20 ℃; for 3h; Inert atmosphere;

2,4,6-trimethylaniline; With pyridine; In dichloromethane; at 20 ℃; for 16h; Inert atmosphere;
DOI:10.1002/anie.201507180

Reference yield:

: 112639-11-9
1,3-dihydroxy-2-iodo-5-methylbenzene

: 1240403-17-1
(2R,2′R)-2,2′-((2-iodo-1,3-phenylene)bis(oxy))bis(N-mesitylpropanamide)

Guidance literature:: Multi-step reaction with 3 steps

1.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 16 h / 20 °C / Inert atmosphere

2.1: sodium hydroxide / tetrahydrofuran; water; methanol / 6 h / 20 °C

3.1: oxalyl dichloride / dichloromethane / 3 h / 20 °C / Inert atmosphere

3.2: 16 h / 20 °C / Inert atmosphere

With oxalyl dichloride; di-isopropyl azodicarboxylate; triphenylphosphine; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water;
DOI:10.1002/anie.201507180