(2R)-1-(tert-butyl(dimethyl)silyloxy)-4-(4-methoxybenzyloxy)-2-methylbutane

Base Information

Chemical Name:(2R)-1-(tert-butyl(dimethyl)silyloxy)-4-(4-methoxybenzyloxy)-2-methylbutane
CAS No.:727411-50-9
Molecular Formula:C₁₉H₃₄O₃Si
Molecular Weight:338.563
Hs Code.:

Synonyms:(2R)-1-(tert-butyl(dimethyl)silyloxy)-4-(4-methoxybenzyloxy)-2-methylbutane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2R)-1-(tert-butyl(dimethyl)silyloxy)-4-(4-methoxybenzyloxy)-2-methylbutane

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Technology Process of (2R)-1-(tert-butyl(dimethyl)silyloxy)-4-(4-methoxybenzyloxy)-2-methylbutane

There total 3 articles about (2R)-1-(tert-butyl(dimethyl)silyloxy)-4-(4-methoxybenzyloxy)-2-methylbutane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 147915-55-7
(3R)-4-(tert-butyldimethylsilanyloxy)-3-methylbutan-1-ol

: 4-methoxybenzyl-2,2,2-trichloroacetimidate

: 727411-50-9
(2R)-1-(tert-butyl(dimethyl)silyloxy)-4-(4-methoxybenzyloxy)-2-methylbutane

Guidance literature:: With pyridinium p-toluenesulfonate; In dichloromethane; at 25 ℃; for 24h;
DOI:10.1071/CH03298

Reference yield:

: 156757-31-2
(3R)-4-(tert-butyldimethylsilanyloxy)-3-methylbutyraldehyde

: 727411-50-9
(2R)-1-(tert-butyl(dimethyl)silyloxy)-4-(4-methoxybenzyloxy)-2-methylbutane

Guidance literature:: Multi-step reaction with 2 steps

1: 9.8 g / NaBH₄; MeOH / 24 h / 25 °C

2: 99 percent / PPTS / CH₂Cl₂ / 24 h / 25 °C

With methanol; sodium tetrahydroborate; pyridinium p-toluenesulfonate; In dichloromethane;
DOI:10.1071/CH03298

Reference yield:

: 172668-98-3
(3R)-4-(tert-butyldimethylsilanyloxy)-3-methylbutyronitrile

: 727411-50-9
(2R)-1-(tert-butyl(dimethyl)silyloxy)-4-(4-methoxybenzyloxy)-2-methylbutane

Guidance literature:: Multi-step reaction with 3 steps

1: DIBAL-H / CH₂Cl₂ / 1 h / -78 °C

2: 9.8 g / NaBH₄; MeOH / 24 h / 25 °C

3: 99 percent / PPTS / CH₂Cl₂ / 24 h / 25 °C

With methanol; sodium tetrahydroborate; pyridinium p-toluenesulfonate; diisobutylaluminium hydride; In dichloromethane;
DOI:10.1071/CH03298