(2-acetamido-5-acetoxybenzyl) diallyl phosphate

Base Information

Chemical Name:(2-acetamido-5-acetoxybenzyl) diallyl phosphate
CAS No.:494763-99-4
Molecular Formula:C₁₇H₂₂NO₇P
Molecular Weight:383.338
Hs Code.:

Synonyms:(2-acetamido-5-acetoxybenzyl) diallyl phosphate

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Chemical Property of (2-acetamido-5-acetoxybenzyl) diallyl phosphate

Chemical Property:

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Technology Process of (2-acetamido-5-acetoxybenzyl) diallyl phosphate

There total 3 articles about (2-acetamido-5-acetoxybenzyl) diallyl phosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: acetic acid 4-acetylamino-3-(bis-allyloxy-phosphanyloxymethyl)-phenyl ester

: 494763-99-4
(2-acetamido-5-acetoxybenzyl) diallyl phosphate

Guidance literature:: With tert.-butylhydroperoxide; In dichloromethane; acetonitrile; at 20 ℃; for 1.5h;
DOI:10.1139/v02-119

Reference yield:

: 53165-19-8
2-acetamido-5-acetoxybenzaldehyde

: 494763-99-4
(2-acetamido-5-acetoxybenzyl) diallyl phosphate

Guidance literature:: Multi-step reaction with 3 steps

1: 60 percent / NaBH₄; potassium dihydrogen phosphate / methanol / 0.5 h

2: 1H-tetrazole / CH₂Cl₂; acetonitrile / 2.5 h / 20 °C

3: 210 mg / tert-butyl hydroperoxide / CH₂Cl₂; acetonitrile; various solvent(s) / 1.5 h / 20 °C

With 1H-tetrazole; tert.-butylhydroperoxide; sodium tetrahydroborate; potassium dihydrogenphosphate; In methanol; dichloromethane; acetonitrile;
DOI:10.1139/v02-119

Reference yield:

: 494763-97-2
4-acetamido-3-hydroxymethylphenyl acetate

: 494763-99-4
(2-acetamido-5-acetoxybenzyl) diallyl phosphate

Guidance literature:: Multi-step reaction with 2 steps

1: 1H-tetrazole / CH₂Cl₂; acetonitrile / 2.5 h / 20 °C

2: 210 mg / tert-butyl hydroperoxide / CH₂Cl₂; acetonitrile; various solvent(s) / 1.5 h / 20 °C

With 1H-tetrazole; tert.-butylhydroperoxide; In dichloromethane; acetonitrile;
DOI:10.1139/v02-119