r-4-t-butyl-c-1-(4,4-dimethyl-3,5-dioxa-2,6-dioxocyclohexyl)-t-1-phenylcyclohexane

Base Information

Chemical Name:r-4-t-butyl-c-1-(4,4-dimethyl-3,5-dioxa-2,6-dioxocyclohexyl)-t-1-phenylcyclohexane
CAS No.:144879-64-1
Molecular Formula:C₂₂H₃₀O₄
Molecular Weight:358.478
Hs Code.:

Synonyms:r-4-t-butyl-c-1-(4,4-dimethyl-3,5-dioxa-2,6-dioxocyclohexyl)-t-1-phenylcyclohexane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of r-4-t-butyl-c-1-(4,4-dimethyl-3,5-dioxa-2,6-dioxocyclohexyl)-t-1-phenylcyclohexane

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Technology Process of r-4-t-butyl-c-1-(4,4-dimethyl-3,5-dioxa-2,6-dioxocyclohexyl)-t-1-phenylcyclohexane

There total 3 articles about r-4-t-butyl-c-1-(4,4-dimethyl-3,5-dioxa-2,6-dioxocyclohexyl)-t-1-phenylcyclohexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2033-24-1
cycl-isopropylidene malonate

: 144879-64-1
r-4-t-butyl-c-1-(4,4-dimethyl-3,5-dioxa-2,6-dioxocyclohexyl)-t-1-phenylcyclohexane

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / AcOH, NH₄OAc, 4 Angstroem molecular sieves / toluene / 3 h

2: 1.) CuCN / 1.) THF, a) 0 deg C, b) room temperature, 30 min, 2.) THF, 0 deg C, overnight

With 4 A molecular sieve; ammonium acetate; acetic acid; In toluene;
DOI:10.1016/S0040-4020(01)89447-3

Reference yield:

: 98-53-3
4-tercbutyl-cyclohexanone

: 144879-64-1
r-4-t-butyl-c-1-(4,4-dimethyl-3,5-dioxa-2,6-dioxocyclohexyl)-t-1-phenylcyclohexane

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / AcOH, NH₄OAc, 4 Angstroem molecular sieves / toluene / 3 h

2: 1.) CuCN / 1.) THF, a) 0 deg C, b) room temperature, 30 min, 2.) THF, 0 deg C, overnight

With 4 A molecular sieve; ammonium acetate; acetic acid; In toluene;
DOI:10.1016/S0040-4020(01)89447-3

Reference yield:

: phenylmagnesium bromide

: 144879-63-0
isopropylidene (4-t-butylcyclohexylidene)malonate

: 144879-64-1
r-4-t-butyl-c-1-(4,4-dimethyl-3,5-dioxa-2,6-dioxocyclohexyl)-t-1-phenylcyclohexane

Guidance literature:: With 1.) CuCN; Yield given. Multistep reaction; 1.) THF, a) 0 deg C, b) room temperature, 30 min, 2.) THF, 0 deg C, overnight;
DOI:10.1016/S0040-4020(01)89447-3