Technology Process of C63H78O3Si
There total 6 articles about C63H78O3Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
copper(l) iodide; triethylamine;
bis-triphenylphosphine-palladium(II) chloride;
In
tetrahydrofuran;
at 20 ℃;
for 6h;
DOI:10.1021/jo070607z
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 98 percent / potassium carbonate; methanol / CH2Cl2 / 6 h / 20 °C
2: 47 percent / triethylamine; CuI / Pd(PPh3)2Cl2 / tetrahydrofuran / 20 °C
3: 92 percent / triethylamine; CuI / Pd(PPh3)2Cl2 / tetrahydrofuran / 6 h / 20 °C
With
methanol; copper(l) iodide; potassium carbonate; triethylamine;
bis-triphenylphosphine-palladium(II) chloride;
In
tetrahydrofuran; dichloromethane;
2: Sonogashira coupling / 3: Sonogashira coupling;
DOI:10.1021/jo070607z
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 100 percent / PPh3; CuI; triethylamine / PdCl2 / 6 h / 20 °C
2: 98 percent / potassium carbonate; methanol / CH2Cl2 / 6 h / 20 °C
3: 47 percent / triethylamine; CuI / Pd(PPh3)2Cl2 / tetrahydrofuran / 20 °C
4: 92 percent / triethylamine; CuI / Pd(PPh3)2Cl2 / tetrahydrofuran / 6 h / 20 °C
With
methanol; copper(l) iodide; potassium carbonate; triethylamine; triphenylphosphine;
bis-triphenylphosphine-palladium(II) chloride; palladium dichloride;
In
tetrahydrofuran; dichloromethane;
1: Sonogashira coupling / 3: Sonogashira coupling / 4: Sonogashira coupling;
DOI:10.1021/jo070607z