Technology Process of 1,2-diamino-4,5-didocosyloxybenzene
There total 4 articles about 1,2-diamino-4,5-didocosyloxybenzene which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
palladium 10% on activated carbon; hydrazine hydrate;
In
ethanol;
for 18h;
Inert atmosphere;
Reflux;
DOI:10.1039/c8tc05580g
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: potassium carbonate / N,N-dimethyl-formamide / 1 h / 20 °C
1.2: 17 h / 80 °C
2.1: nitric acid / water; acetic acid / 60 °C
2.2: 48 h / 20 °C
3.1: hydrazine hydrate; palladium 10% on activated carbon / ethanol / 18 h / Inert atmosphere; Reflux
With
palladium 10% on activated carbon; nitric acid; potassium carbonate; hydrazine hydrate;
In
ethanol; water; acetic acid; N,N-dimethyl-formamide;
DOI:10.1039/c8tc05580g
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: nitric acid / water; acetic acid / 60 °C
1.2: 48 h / 20 °C
2.1: hydrazine hydrate; palladium 10% on activated carbon / ethanol / 18 h / Inert atmosphere; Reflux
With
palladium 10% on activated carbon; nitric acid; hydrazine hydrate;
In
ethanol; water; acetic acid;
DOI:10.1039/c8tc05580g
