Technology Process of C37H54N4O7
There total 7 articles about C37H54N4O7 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
palladium on activated charcoal; hydrogen;
In
ethanol;
for 6h;
DOI:10.1021/ol300987d
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: trifluoroacetic acid / dichloromethane / 0.5 h / Cooling with ice
1.2: pH 12
2.1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / N,N-dimethyl-formamide / 0.08 h / 0 °C
2.2: 4 h / 20 °C
3.1: palladium on activated charcoal; hydrogen / ethanol / 6 h
With
palladium on activated charcoal; hydrogen; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; trifluoroacetic acid;
In
ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ol300987d
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / N,N-dimethyl-formamide / 0.08 h / 0 °C
1.2: 6 h / 20 °C
2.1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / N,N-dimethyl-formamide / 0.08 h / 0 °C
2.2: 4 h / 20 °C
3.1: palladium on activated charcoal; hydrogen / ethanol / 6 h
With
palladium on activated charcoal; hydrogen; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate;
In
ethanol; N,N-dimethyl-formamide;
DOI:10.1021/ol300987d