6-chloro-2-hydroxy-N-methoxy-N-methyl-3-{2-[(R)-1-((2R,5R)-5-methyl-tetrahydro-furan-2-yl)-propylamino]-3,4-dioxo-cyclobut-1-enylamino}-benzene sulfonamide

Base Information

• Chemical Name: 6-chloro-2-hydroxy-N-methoxy-N-methyl-3-{2-[(R)-1-((2R,5R)-5-methyl-tetrahydro-furan-2-yl)-propylamino]-3,4-dioxo-cyclobut-1-enylamino}-benzene sulfonamide
• CAS No.: 1206894-97-4
• Molecular Formula: C₂₀H₂₆ClN₃O₇S
• Molecular Weight: 487.961

Synonyms:6-chloro-2-hydroxy-N-methoxy-N-methyl-3-{2-[(R)-1-((2R,5R)-5-methyl-tetrahydro-furan-2-yl)-propylamino]-3,4-dioxo-cyclobut-1-enylamino}-benzene sulfonamide

Chemical Property of 6-chloro-2-hydroxy-N-methoxy-N-methyl-3-{2-[(R)-1-((2R,5R)-5-methyl-tetrahydro-furan-2-yl)-propylamino]-3,4-dioxo-cyclobut-1-enylamino}-benzene sulfonamide

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Technology Process of 6-chloro-2-hydroxy-N-methoxy-N-methyl-3-{2-[(R)-1-((2R,5R)-5-methyl-tetrahydro-furan-2-yl)-propylamino]-3,4-dioxo-cyclobut-1-enylamino}-benzene sulfonamide

There total 1 articles about 6-chloro-2-hydroxy-N-methoxy-N-methyl-3-{2-[(R)-1-((2R,5R)-5-methyl-tetrahydro-furan-2-yl)-propylamino]-3,4-dioxo-cyclobut-1-enylamino}-benzene sulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(R)-1-((2R,5R)-5-methyltetrahydrofuran-2-yl)propylamine para-toluenesulfonate salt (1092389-32-6) + 6-chloro-3-((2-ethoxy-3,4-dioxocyclobut-1-en-1-yl)-amino)-2-hydroxy-N-methoxy-N-methylbenzenesulfonamide (1206896-19-6) → 6-chloro-2-hydroxy-N-methoxy-N-methyl-3-{2-[(R)-1-((2R,5R)-5-methyl-tetrahydro-furan-2-yl)-propylamino]-3,4-dioxo-cyclobut-1-enylamino}-benzene sulfonamide (1206894-97-4)

Guidance literature:

With triethylamine; In ethanol; acetonitrile; at 20 - 60 ℃; Inert atmosphere;

Reference yield:

6-chloro-2-hydroxy-N-methoxy-N-methyl-3-{2-[(R)-1-((2R,5R)-5-methyl-tetrahydro-furan-2-yl)-propylamino]-3,4-dioxo-cyclobut-1-enylamino}-benzene sulfonamide (1206894-97-4) + cholin hydroxide (123-41-1) → 3-chloro-2-(methoxy-methyl-sulfamoyl)-6-{2-[(R)-1-((2R,5R)-5-methyl-tetrahydro-furan-2-yl)-propylamino]-3,4-dioxo-cyclobut-1-enylamino}-phenolate(2-hydroxy-ethyl)-trimethyl-ammonium (1314798-70-3)

Guidance literature:

In methanol; ethyl acetate; isopropyl alcohol; for 0.333333h; Reflux;

upstream raw materials:

(R)-1-((2R,5R)-5-methyltetrahydrofuran-2-yl)propylamine para-toluenesulfonate salt

6-chloro-3-((2-ethoxy-3,4-dioxocyclobut-1-en-1-yl)-amino)-2-hydroxy-N-methoxy-N-methylbenzenesulfonamide

Downstream raw materials:

3-chloro-2-(methoxy-methyl-sulfamoyl)-6-{2-[(R)-1-((2R,5R)-5-methyl-tetrahydro-furan-2-yl)-propylamino]-3,4-dioxo-cyclobut-1-enylamino}-phenolate(2-hydroxy-ethyl)-trimethyl-ammonium

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