2-(4-methyl-benzoyl)-4,5-(methylenedioxy)-phenylacetic acid methyl ester

Base Information

• Chemical Name: 2-(4-methyl-benzoyl)-4,5-(methylenedioxy)-phenylacetic acid methyl ester
• CAS No.: 197369-10-1
• Molecular Formula: C₁₈H₁₆O₅
• Molecular Weight: 312.322

Synonyms:2-(4-methyl-benzoyl)-4,5-(methylenedioxy)-phenylacetic acid methyl ester

Chemical Property of 2-(4-methyl-benzoyl)-4,5-(methylenedioxy)-phenylacetic acid methyl ester

Chemical Property:

Purity/Quality:

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Technology Process of 2-(4-methyl-benzoyl)-4,5-(methylenedioxy)-phenylacetic acid methyl ester

There total 2 articles about 2-(4-methyl-benzoyl)-4,5-(methylenedioxy)-phenylacetic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 18.0%

benzo[1,3]dioxol-5-yl-acetic acid methyl ester (326-59-0) + 4-methyl-benzoyl chloride (874-60-2) → 2-(4-methyl-benzoyl)-4,5-(methylenedioxy)-phenylacetic acid methyl ester (197369-10-1)

Guidance literature:

With tin(IV) chloride; In dichloromethane; for 24h; Ambient temperature;

DOI:10.1021/jm980168j

Reference yield:

→ 2-(4-methyl-benzoyl)-4,5-(methylenedioxy)-phenylacetic acid methyl ester (197369-10-1)

Guidance literature:

Reference yield: 52.0%

2-(4-methyl-benzoyl)-4,5-(methylenedioxy)-phenylacetic acid methyl ester (197369-10-1) → 7,8-methylenedioxy-1-(4-methylphenyl)-3,5-dihydro-2,3-benzodiazepin-4(4H)-one

Guidance literature:

With hydrazine hydrate; acetic acid; In ethanol; for 120h; Heating;

DOI:10.1021/jm980168j

upstream raw materials:

benzo[1,3]dioxol-5-yl-acetic acid methyl ester

4-methyl-benzoyl chloride

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