7-(3.5-Dimethoxy-phenylacetoxy)-octansaeure-benzylester

Base Information

Chemical Name:7-(3.5-Dimethoxy-phenylacetoxy)-octansaeure-benzylester
CAS No.:16209-13-5
Molecular Formula:C₂₅H₃₂O₆
Molecular Weight:428.525
Hs Code.:

Synonyms:7-(3.5-Dimethoxy-phenylacetoxy)-octansaeure-benzylester

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Chemical Property of 7-(3.5-Dimethoxy-phenylacetoxy)-octansaeure-benzylester

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Technology Process of 7-(3.5-Dimethoxy-phenylacetoxy)-octansaeure-benzylester

There total 10 articles about 7-(3.5-Dimethoxy-phenylacetoxy)-octansaeure-benzylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 6652-32-0
3,5-dimethoxybenzylchloride

: 16209-10-2
7-Hydroxy-octanoic acid benzyl ester

: 16209-13-5
7-(3.5-Dimethoxy-phenylacetoxy)-octansaeure-benzylester

Guidance literature:: With sodium acetate; triphenylphosphine; palladium dichloride; In benzene; at 100 ℃; for 36h; under 7600 Torr;
DOI:10.1016/0040-4039(80)80207-3

Reference yield:

: 68231-78-7
7-oxooct-2E-enyl acetate

: 16209-13-5
7-(3.5-Dimethoxy-phenylacetoxy)-octansaeure-benzylester

Guidance literature:: Multi-step reaction with 6 steps

1: aq. KOH

2: 85 percent / hydrogen / Pd/C / ethanol

3: CrO₃

4: NaH / hexamethylphosphoric acid triamide / 0 °C

5: 90 percent / NaBH₄ / ethanol

6: 70 percent / PdCl₂, triphenylphosphine, NaOAc / benzene / 36 h / 100 °C / 7600 Torr

With chromium(VI) oxide; potassium hydroxide; sodium tetrahydroborate; hydrogen; sodium acetate; sodium hydride; triphenylphosphine; palladium dichloride; palladium on activated charcoal; In N,N,N,N,N,N-hexamethylphosphoric triamide; ethanol; benzene;
DOI:10.1016/0040-4039(80)80207-3

Reference yield:

: 75320-59-1
7-oxooct-2E-en-1-ol

: 16209-13-5
7-(3.5-Dimethoxy-phenylacetoxy)-octansaeure-benzylester

Guidance literature:: Multi-step reaction with 5 steps

1: 85 percent / hydrogen / Pd/C / ethanol

2: CrO₃

3: NaH / hexamethylphosphoric acid triamide / 0 °C

4: 90 percent / NaBH₄ / ethanol

5: 70 percent / PdCl₂, triphenylphosphine, NaOAc / benzene / 36 h / 100 °C / 7600 Torr

With chromium(VI) oxide; sodium tetrahydroborate; hydrogen; sodium acetate; sodium hydride; triphenylphosphine; palladium dichloride; palladium on activated charcoal; In N,N,N,N,N,N-hexamethylphosphoric triamide; ethanol; benzene;
DOI:10.1016/0040-4039(80)80207-3