N-t-butoxycarbonyl-L-leucyl-Ψ(CH2S)-L-alanyl-α-azanorvaline benzyl ester

Base Information

Chemical Name:N-t-butoxycarbonyl-L-leucyl-Ψ(CH2S)-L-alanyl-α-azanorvaline benzyl ester
CAS No.:112383-34-3
Molecular Formula:C₂₅H₄₁N₃O₅S
Molecular Weight:495.684
Hs Code.:

Synonyms:N-t-butoxycarbonyl-L-leucyl-Ψ(CH2S)-L-alanyl-α-azanorvaline benzyl ester

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Chemical Property of N-t-butoxycarbonyl-L-leucyl-Ψ(CH2S)-L-alanyl-α-azanorvaline benzyl ester

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Technology Process of N-t-butoxycarbonyl-L-leucyl-Ψ(CH2S)-L-alanyl-α-azanorvaline benzyl ester

There total 6 articles about N-t-butoxycarbonyl-L-leucyl-Ψ(CH2S)-L-alanyl-α-azanorvaline benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 112383-33-2
2-(2-t-butoxycarbonylamino-4-methylpenthylthio)propionic acid

: 112383-15-0
α-azanorvaline benzyl ester hydrochloride

: 112383-34-3
N-t-butoxycarbonyl-L-leucyl-Ψ(CH2S)-L-alanyl-α-azanorvaline benzyl ester

Guidance literature:: With benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide;

Reference yield:

: 82010-31-9
(S)-(1-hydroxymethyl-3-methylbutyl)carbamic acid tert-butyl ester

: 112383-34-3
N-t-butoxycarbonyl-L-leucyl-Ψ(CH2S)-L-alanyl-α-azanorvaline benzyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 89 percent / pyridine / 4 °C

2: dimethylformamide / 4 h / 45 - 50 °C

3: 100 g / ethylenediamine / 3 h

4: 34 percent / triethylamine / dimethylformamide; H₂O / 31 h

5: 66 percent / 1-hydroxybenzotriazole, dicyclohexylcarbodi-imide, triethylamine / dimethylformamide

With benzotriazol-1-ol; ethylenediamine; triethylamine; dicyclohexyl-carbodiimide; In pyridine; water; N,N-dimethyl-formamide;

Reference yield:

: 112157-38-7
tert-butyl (S)-(1-mercapto-4-methylpentan-2-yl)carbamate

: 112383-34-3
N-t-butoxycarbonyl-L-leucyl-Ψ(CH2S)-L-alanyl-α-azanorvaline benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 34 percent / triethylamine / dimethylformamide; H₂O / 31 h

2: 66 percent / 1-hydroxybenzotriazole, dicyclohexylcarbodi-imide, triethylamine / dimethylformamide

With benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; In water; N,N-dimethyl-formamide;