[Mn(CO)2(P(OC₆H₅)3)2((C₃N₂H₃)2)]⁽¹⁺⁾*ClO₄^(1-) = [Mn(CO)2(P(OC₆H₅)3)2((C₃N₂H₃)2)]ClO₄

Base Information

• Chemical Name: [Mn(CO)2(P(OC₆H₅)3)2((C₃N₂H₃)2)]⁽¹⁺⁾*ClO₄^(1-) = [Mn(CO)2(P(OC₆H₅)3)2((C₃N₂H₃)2)]ClO₄
• CAS No.: 107528-65-4
• Molecular Formula: C₄₄H₃₆MnN₄O₈P₂*ClO₄
• Molecular Weight: 965.128

Synonyms:[Mn(CO)2(P(OC₆H₅)3)2((C₃N₂H₃)2)]⁽¹⁺⁾*ClO₄^(1-) = [Mn(CO)2(P(OC₆H₅)3)2((C₃N₂H₃)2)]ClO₄

Chemical Property of [Mn(CO)2(P(OC₆H₅)3)2((C₃N₂H₃)2)]⁽¹⁺⁾*ClO₄^(1-) = [Mn(CO)2(P(OC₆H₅)3)2((C₃N₂H₃)2)]ClO₄

Chemical Property:

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Technology Process of [Mn(CO)2(P(OC₆H₅)3)2((C₃N₂H₃)2)]⁽¹⁺⁾*ClO₄^(1-) = [Mn(CO)2(P(OC₆H₅)3)2((C₃N₂H₃)2)]ClO₄

There total 2 articles about [Mn(CO)2(P(OC₆H₅)3)2((C₃N₂H₃)2)]⁽¹⁺⁾*ClO₄^(1-) = [Mn(CO)2(P(OC₆H₅)3)2((C₃N₂H₃)2)]ClO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

[Mn(CO)2(P(OC6H5)3)2((C3N2H3)(C3N2H2))] (107478-99-9) → [Mn(CO)2(P(OC6H5)3)2((C3N2H3)2)](1+)*ClO4(1-) = [Mn(CO)2(P(OC6H5)3)2((C3N2H3)2)]ClO4 (107528-65-4)

Guidance literature:

With HClO₄; In dichloromethane; (Ar); stirred (room temp., 1 h); filtered (Celite); concd. (reduced pressure); pptd. by addition of hexane; elem. anal.;

DOI:10.1016/0022-328X(86)80173-5

Reference yield:

triphenyl phosphite (101-02-0) + 2,2'-biimidazole (492-98-8) → [Mn(CO)2(P(OC6H5)3)2((C3N2H3)2)](1+)*ClO4(1-) = [Mn(CO)2(P(OC6H5)3)2((C3N2H3)2)]ClO4 (107528-65-4)

Guidance literature:

Multi-step reaction with 2 steps

1: KOH / tetrahydrofuran

2: HClO₄ / dichloromethane

With KOH; HClO₄; In tetrahydrofuran; dichloromethane;

DOI:10.1016/0022-328X(86)80173-5

upstream raw materials:

[Mn(CO)2(P(OC₆H₅)3)2((C₃N₂H₃)(C₃N₂H₂))]

triphenyl phosphite

2,2'-biimidazole

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