(1R,2R,3S,4R,5R,6R)-3-ammonio-1,2,4,5,6-pentahydroxycyclohexanecarboxylate

Base Information

Chemical Name:(1R,2R,3S,4R,5R,6R)-3-ammonio-1,2,4,5,6-pentahydroxycyclohexanecarboxylate
CAS No.:1301703-41-2
Molecular Formula:C₇H₁₃NO₇
Molecular Weight:223.183
Hs Code.:

Synonyms:(1R,2R,3S,4R,5R,6R)-3-ammonio-1,2,4,5,6-pentahydroxycyclohexanecarboxylate

Suppliers and Price of (1R,2R,3S,4R,5R,6R)-3-ammonio-1,2,4,5,6-pentahydroxycyclohexanecarboxylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (1R,2R,3S,4R,5R,6R)-3-ammonio-1,2,4,5,6-pentahydroxycyclohexanecarboxylate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (1R,2R,3S,4R,5R,6R)-3-ammonio-1,2,4,5,6-pentahydroxycyclohexanecarboxylate

There total 6 articles about (1R,2R,3S,4R,5R,6R)-3-ammonio-1,2,4,5,6-pentahydroxycyclohexanecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1301703-46-7
(3aS,4R,5R,6R,7S,7aR)-7-ammonio-4,5,6-trihydroxy-2,2-dimethylhexahydrobenzo[d][1,3]dioxole-3a-carboxylate

: 1301703-41-2
(1R,2R,3S,4R,5R,6R)-3-ammonio-1,2,4,5,6-pentahydroxycyclohexanecarboxylate

Guidance literature:: With hydrogenchloride; In water; at 20 ℃; for 24h; Inert atmosphere;
DOI:10.1039/c1cc10643k

Reference yield:

: 1301703-43-4
(3aR,4R,5R,6R,7S,7aR)-dibenzyl 5,6-dihydroxy-2,2-dimethylhexahydro-4,7-(epoxyimino)benzo[d][1,3]dioxole-3a,8-dicarboxylate

: 1301703-41-2
(1R,2R,3S,4R,5R,6R)-3-ammonio-1,2,4,5,6-pentahydroxycyclohexanecarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: palladium 10% on activated carbon; hydrogen / methanol / 24 h / 20 °C / Inert atmosphere

2: hydrogenchloride / water / 24 h / 20 °C / Inert atmosphere

With hydrogenchloride; palladium 10% on activated carbon; hydrogen; In methanol; water;
DOI:10.1039/c1cc10643k

Reference yield:

: 1301703-27-4
(3aS,7aR)-benzyl 2,2-dimethyl-3a,7a-dihydrobenzo[d][1,3]dioxole-3a-carboxylate

: 1301703-41-2
(1R,2R,3S,4R,5R,6R)-3-ammonio-1,2,4,5,6-pentahydroxycyclohexanecarboxylate

Guidance literature:: Multi-step reaction with 4 steps

1: tetrabutylammonium periodite / dichloromethane / 2 h / -78 - 20 °C / Inert atmosphere

2: osmium(VIII) oxide; 4-methylmorpholine N-oxide / water; acetone; tert-butyl alcohol / 24 h / 20 °C / Inert atmosphere

3: palladium 10% on activated carbon; hydrogen / methanol / 24 h / 20 °C / Inert atmosphere

4: hydrogenchloride / water / 24 h / 20 °C / Inert atmosphere

With hydrogenchloride; osmium(VIII) oxide; palladium 10% on activated carbon; hydrogen; tetrabutylammonium periodite; 4-methylmorpholine N-oxide; In methanol; dichloromethane; water; acetone; tert-butyl alcohol;
DOI:10.1039/c1cc10643k