3-((4R,5S)-2-(4-methoxyphenyl)-4-methyl-5-vinyl-1,3-dioxolan-4-yl)propanal

Base Information

Chemical Name:3-((4R,5S)-2-(4-methoxyphenyl)-4-methyl-5-vinyl-1,3-dioxolan-4-yl)propanal
CAS No.:1403584-89-3
Molecular Formula:C₁₆H₂₀O₄
Molecular Weight:276.332
Hs Code.:

Synonyms:3-((4R,5S)-2-(4-methoxyphenyl)-4-methyl-5-vinyl-1,3-dioxolan-4-yl)propanal

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Chemical Property of 3-((4R,5S)-2-(4-methoxyphenyl)-4-methyl-5-vinyl-1,3-dioxolan-4-yl)propanal

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Technology Process of 3-((4R,5S)-2-(4-methoxyphenyl)-4-methyl-5-vinyl-1,3-dioxolan-4-yl)propanal

There total 4 articles about 3-((4R,5S)-2-(4-methoxyphenyl)-4-methyl-5-vinyl-1,3-dioxolan-4-yl)propanal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 3-((4R,5S)-2-(4-methoxyphenyl)-4-methyl-5-vinyl-1,3-dioxolan-4-yl)propan-1-ol

: 1403584-89-3
3-((4R,5S)-2-(4-methoxyphenyl)-4-methyl-5-vinyl-1,3-dioxolan-4-yl)propanal

Guidance literature:: With sodium hypochlorite; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; sodium hydrogencarbonate; potassium bromide; In dichloromethane; water; at 0 - 20 ℃; for 3h; pH=9; Reagent/catalyst; Solvent; Temperature;

Reference yield:

: 1403584-86-0
(8S,9S)-14,14,15,15-tetramethyl-8-vinyl-2,5,7,13-tetraoxa-14-silahexadecan-9-one

: 1403584-89-3
3-((4R,5S)-2-(4-methoxyphenyl)-4-methyl-5-vinyl-1,3-dioxolan-4-yl)propanal

Guidance literature:: Multi-step reaction with 3 steps

1.1: tetrahydrofuran; diethyl ether / 18 h / -94 - 20 °C

2.1: carbon tetrabromide; 1H-imidazole / isopropyl alcohol / Reflux

2.2: 2.17 h / 20 °C / Inert atmosphere

3.1: sodium hydrogencarbonate; potassium bromide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; sodium hypochlorite / dichloromethane; water / 3 h / 0 - 20 °C / pH 9

With 1H-imidazole; sodium hypochlorite; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; carbon tetrabromide; sodium hydrogencarbonate; potassium bromide; In tetrahydrofuran; diethyl ether; dichloromethane; water; isopropyl alcohol;

Reference yield:

: 1403584-85-9
(8S,9S)-14,14,15,15-tetramethyl-8-vinyl-2,5,7,13-tetraoxa-14-silahexadecan-9-ol

: 1403584-89-3
3-((4R,5S)-2-(4-methoxyphenyl)-4-methyl-5-vinyl-1,3-dioxolan-4-yl)propanal

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydrogencarbonate; potassium bromide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; sodium hypochlorite / dichloromethane; water / 2 h / 0 - 20 °C / pH 9

2.1: tetrahydrofuran; diethyl ether / 18 h / -94 - 20 °C

3.1: carbon tetrabromide; 1H-imidazole / isopropyl alcohol / Reflux

3.2: 2.17 h / 20 °C / Inert atmosphere

4.1: sodium hydrogencarbonate; potassium bromide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; sodium hypochlorite / dichloromethane; water / 3 h / 0 - 20 °C / pH 9

With 1H-imidazole; sodium hypochlorite; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; carbon tetrabromide; sodium hydrogencarbonate; potassium bromide; In tetrahydrofuran; diethyl ether; dichloromethane; water; isopropyl alcohol;