ethyl trithiocarbonate

Base Information

Chemical Name:ethyl trithiocarbonate
CAS No.:75401-07-9
Molecular Formula:C₃₃H₂₉N₂O₅PS₃
Molecular Weight:660.775
Hs Code.:

ethyl <N-(p-nitrobenzyloxycarbonyl-triphenylphosphoranylidene-methyl)-2-oxo-azetidin-4-yl> trithiocarbonate

Synonyms:ethyl trithiocarbonate

Suppliers and Price of ethyl trithiocarbonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethyl trithiocarbonate

Chemical Property:

Purity/Quality:

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Technology Process of ethyl trithiocarbonate

There total 3 articles about ethyl trithiocarbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 603-35-0
triphenylphosphine

: 69077-80-1
Chloro-(2-ethylsulfanylthiocarbonylsulfanyl-4-oxo-azetidin-1-yl)-acetic acid 4-nitro-benzyl ester

: 75401-07-9
ethyl trithiocarbonate

Guidance literature:: With polymeric Huenig base; In 1,4-dioxane; at 50 ℃; for 15h; Yield given;
DOI:10.1002/hlca.19800630436

Reference yield:

: 75388-67-9
ethyl 2-oxo-azetidin-4-yl trithiocarbonate

: 75401-07-9
ethyl trithiocarbonate

Guidance literature:: Multi-step reaction with 3 steps

1: 88 percent / mol. sieves 3 or 4 Angstroem / toluene; dimethylformamide / 1) RT, overnight, 2) 50 deg C, 2 h

2: SOCl₂, polymeric Huenig base / dioxane / 3 h / Ambient temperature

3: polymeric Huenig base / dioxane / 15 h / 50 °C

With thionyl chloride; 3 A molecular sieve; polymeric Huenig base; In 1,4-dioxane; N,N-dimethyl-formamide; toluene;
DOI:10.1002/hlca.19800630436

Reference yield:

: 69077-79-8
2-[(4R,S)-ethylthiothiocarbonylthio-2-oxo-1-azetidinyl]-2-hydroxyacetic acid p-nitrobenzyl ester

: 75401-07-9
ethyl trithiocarbonate

Guidance literature:: Multi-step reaction with 2 steps

1: SOCl₂, polymeric Huenig base / dioxane / 3 h / Ambient temperature

2: polymeric Huenig base / dioxane / 15 h / 50 °C

With thionyl chloride; polymeric Huenig base; In 1,4-dioxane;
DOI:10.1002/hlca.19800630436