Benzyl (S)-2-hydroxy-N-(2,3,6-tri-O-acetyl-4-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-β-D-glucopyranosyl)succinate

Base Information

Chemical Name:Benzyl (S)-2-hydroxy-N-(2,3,6-tri-O-acetyl-4-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-β-D-glucopyranosyl)succinate
CAS No.:309730-49-2
Molecular Formula:C₃₇H₄₇NO₂₁
Molecular Weight:841.774
Hs Code.:

Synonyms:Benzyl (S)-2-hydroxy-N-(2,3,6-tri-O-acetyl-4-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-β-D-glucopyranosyl)succinate

Suppliers and Price of Benzyl (S)-2-hydroxy-N-(2,3,6-tri-O-acetyl-4-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-β-D-glucopyranosyl)succinate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Benzyl (S)-2-hydroxy-N-(2,3,6-tri-O-acetyl-4-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-β-D-glucopyranosyl)succinate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Benzyl (S)-2-hydroxy-N-(2,3,6-tri-O-acetyl-4-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-β-D-glucopyranosyl)succinate

There total 3 articles about Benzyl (S)-2-hydroxy-N-(2,3,6-tri-O-acetyl-4-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-β-D-glucopyranosyl)succinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 309730-46-9
Benzyl (S)-2-tert-butyldimethylsilyloxy-N-(2,3,6-tri-O-acetyl-4-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-β-D-glucopyranosyl)succinate

: 309730-49-2
Benzyl (S)-2-hydroxy-N-(2,3,6-tri-O-acetyl-4-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-β-D-glucopyranosyl)succinate

Guidance literature:: With boron trifluoride diethyl etherate; In chloroform; at 20 ℃; for 1.5h;

Reference yield:

: 59044-96-1,93079-64-2,120575-75-9,30854-63-8
2,3,6-tri-O-acetyl-4-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-β-D-glucopyranosylamine

: 309730-49-2
Benzyl (S)-2-hydroxy-N-(2,3,6-tri-O-acetyl-4-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-β-D-glucopyranosyl)succinate

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / HBTU; i-Pr₂NEt / dimethylformamide

2: 85 percent / BF₃*OEt₂ / CHCl₃ / 1.5 h / 20 °C

With boron trifluoride diethyl etherate; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In chloroform; N,N-dimethyl-formamide; 1: glycosylation / 2: desilylation;

Reference yield:

: 309730-43-6
benzyl hydrogen (S)-2-(tert-butyldimethylsilyloxy)succinate

: 309730-49-2
Benzyl (S)-2-hydroxy-N-(2,3,6-tri-O-acetyl-4-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-β-D-glucopyranosyl)succinate

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / HBTU; i-Pr₂NEt / dimethylformamide

2: 85 percent / BF₃*OEt₂ / CHCl₃ / 1.5 h / 20 °C

With boron trifluoride diethyl etherate; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In chloroform; N,N-dimethyl-formamide; 1: glycosylation / 2: desilylation;