carbonic acid 2-(methoxy-methyl-carbamoyl)-cyclohex-2-enyl ester methyl ester

Base Information

Chemical Name:carbonic acid 2-(methoxy-methyl-carbamoyl)-cyclohex-2-enyl ester methyl ester
CAS No.:932743-53-8
Molecular Formula:C₁₁H₁₇NO₅
Molecular Weight:243.26
Hs Code.:

Synonyms:carbonic acid 2-(methoxy-methyl-carbamoyl)-cyclohex-2-enyl ester methyl ester

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Chemical Property of carbonic acid 2-(methoxy-methyl-carbamoyl)-cyclohex-2-enyl ester methyl ester

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Technology Process of carbonic acid 2-(methoxy-methyl-carbamoyl)-cyclohex-2-enyl ester methyl ester

There total 2 articles about carbonic acid 2-(methoxy-methyl-carbamoyl)-cyclohex-2-enyl ester methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 932743-81-2
6-hydroxy-cyclohex-1-enecarboxylic acid methoxy-methyl-amide

: 79-22-1
methyl chloroformate

: 932743-53-8
carbonic acid 2-(methoxy-methyl-carbamoyl)-cyclohex-2-enyl ester methyl ester

Guidance literature:: With dmap; In pyridine; chloroform; at 20 ℃; for 2h;
DOI:10.1021/ol0700207

Reference yield:

: 865780-25-2
methyl 6-hydroxy-cyclohex-1-enecarboxylate

: 932743-53-8
carbonic acid 2-(methoxy-methyl-carbamoyl)-cyclohex-2-enyl ester methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: aq. KOH / propan-2-ol / 4 h / 50 °C

1.2: 81 percent / Et₃N; WSCI / CH₂Cl₂ / 10 h / 20 °C

2.1: DMAP / CHCl₃; pyridine / 2 h / 20 °C

With dmap; potassium hydroxide; In pyridine; chloroform; isopropyl alcohol;
DOI:10.1021/ol0700207

Reference yield: 98.0%

: 932743-53-8
carbonic acid 2-(methoxy-methyl-carbamoyl)-cyclohex-2-enyl ester methyl ester

: 100-46-9
benzylamine

: 932743-66-3
6-benzylamino-cyclohex-1-enecarboxylic acid methoxy-methyl-amide

Guidance literature:: With benzenesulfonamide; chiral diaminophosphine oxide; bis(η3-allyl-μ-chloropalladium(II)); In acetonitrile; at -30 ℃; for 32h;
DOI:10.1021/ol0700207