2-pivaloylamino-5-triisopropylsilyloxyphenylboronic acid

Base Information

Chemical Name:2-pivaloylamino-5-triisopropylsilyloxyphenylboronic acid
CAS No.:1421005-59-5
Molecular Formula:C₂₀H₃₆BNO₄Si
Molecular Weight:393.407
Hs Code.:

Synonyms:2-pivaloylamino-5-triisopropylsilyloxyphenylboronic acid

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Chemical Property of 2-pivaloylamino-5-triisopropylsilyloxyphenylboronic acid

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Technology Process of 2-pivaloylamino-5-triisopropylsilyloxyphenylboronic acid

There total 3 articles about 2-pivaloylamino-5-triisopropylsilyloxyphenylboronic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 1421005-58-4
N-(4-(triisopropylsilyloxy)phenyl)pivalamide

: 1421005-59-5
2-pivaloylamino-5-triisopropylsilyloxyphenylboronic acid

Guidance literature:: N-(4-(triisopropylsilyloxy)phenyl)pivalamide; With tert.-butyl lithium; In diethyl ether; pentane; at -15 - -10 ℃; for 3h; Inert atmosphere;

With Trimethyl borate; In diethyl ether; pentane; at 20 ℃; Inert atmosphere;
DOI:10.1016/j.bmc.2012.11.011

Reference yield:

: 13154-24-0
triisopropylsilyl chloride

: 1421005-59-5
2-pivaloylamino-5-triisopropylsilyloxyphenylboronic acid

Guidance literature:: Multi-step reaction with 3 steps

1.1: 1H-imidazole / dichloromethane / 5.42 h / Inert atmosphere

2.1: triethylamine / tetrahydrofuran; diethyl ether / 1 h / 0 °C / Inert atmosphere

3.1: tert.-butyl lithium / diethyl ether; pentane / 3 h / -15 - -10 °C / Inert atmosphere

3.2: 20 °C / Inert atmosphere

With 1H-imidazole; tert.-butyl lithium; triethylamine; In tetrahydrofuran; diethyl ether; dichloromethane; pentane;
DOI:10.1016/j.bmc.2012.11.011

Reference yield:

: 123-30-8
4-amino-phenol

: 1421005-59-5
2-pivaloylamino-5-triisopropylsilyloxyphenylboronic acid

Guidance literature:: Multi-step reaction with 3 steps

1.1: 1H-imidazole / dichloromethane / 5.42 h / Inert atmosphere

2.1: triethylamine / tetrahydrofuran; diethyl ether / 1 h / 0 °C / Inert atmosphere

3.1: tert.-butyl lithium / diethyl ether; pentane / 3 h / -15 - -10 °C / Inert atmosphere

3.2: 20 °C / Inert atmosphere

With 1H-imidazole; tert.-butyl lithium; triethylamine; In tetrahydrofuran; diethyl ether; dichloromethane; pentane;
DOI:10.1016/j.bmc.2012.11.011