C₂₆H₂₉N₃O₅S

Base Information

Chemical Name:C₂₆H₂₉N₃O₅S
CAS No.:1356846-60-0
Molecular Formula:C₂₆H₂₉N₃O₅S
Molecular Weight:495.599
Hs Code.:

C<sub>26</sub>H<sub>29</sub>N<sub>3</sub>O<sub>5</sub>S

Synonyms:C₂₆H₂₉N₃O₅S

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₆H₂₉N₃O₅S

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Technology Process of C₂₆H₂₉N₃O₅S

There total 4 articles about C₂₆H₂₉N₃O₅S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 851394-73-5
C₂₇H₃₁N₃O₅S

: 1356846-60-0
C₂₆H₂₉N₃O₅S

Guidance literature:: With lithium hydroxide; In methanol; water; at 20 ℃;
DOI:10.1021/ja209641t

Reference yield:

: 104504-43-0
N-tert-butoxycarbonyl-(S)-3-(4-benzoylphenyl)alanine

: 1356846-60-0
C₂₆H₂₉N₃O₅S

Guidance literature:: Multi-step reaction with 4 steps

1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 24 h / 20 °C / Inert atmosphere

2: trifluoroacetic acid / dichloromethane / 1 h / 20 °C

3: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 4 h / 20 °C / Inert atmosphere

4: lithium hydroxide / methanol; water / 20 °C

With dmap; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; lithium hydroxide; In methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/ja209641t

Reference yield:

: 4-benzoyl-L-phenylalanyltyrosine methyl ester

: 1356846-60-0
C₂₆H₂₉N₃O₅S

Guidance literature:: Multi-step reaction with 2 steps

1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 4 h / 20 °C / Inert atmosphere

2: lithium hydroxide / methanol; water / 20 °C

With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; lithium hydroxide; In methanol; water; N,N-dimethyl-formamide;
DOI:10.1021/ja209641t