piperidine-3-carboxylic acid [2-(3,4-dibenzyloxy-5-oxo-2,5-dihydrofuran-2(R)-yl)-2(S)-hydroxyethyl] ester

Base Information

Chemical Name:piperidine-3-carboxylic acid [2-(3,4-dibenzyloxy-5-oxo-2,5-dihydrofuran-2(R)-yl)-2(S)-hydroxyethyl] ester
CAS No.:400844-95-3
Molecular Formula:C₂₆H₂₉NO₇
Molecular Weight:467.519
Hs Code.:

Synonyms:piperidine-3-carboxylic acid [2-(3,4-dibenzyloxy-5-oxo-2,5-dihydrofuran-2(R)-yl)-2(S)-hydroxyethyl] ester

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Chemical Property of piperidine-3-carboxylic acid [2-(3,4-dibenzyloxy-5-oxo-2,5-dihydrofuran-2(R)-yl)-2(S)-hydroxyethyl] ester

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Technology Process of piperidine-3-carboxylic acid [2-(3,4-dibenzyloxy-5-oxo-2,5-dihydrofuran-2(R)-yl)-2(S)-hydroxyethyl] ester

There total 2 articles about piperidine-3-carboxylic acid [2-(3,4-dibenzyloxy-5-oxo-2,5-dihydrofuran-2(R)-yl)-2(S)-hydroxyethyl] ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 400844-87-3
N-(tert-butyloxycarbonyl)piperidine-3-carboxylic acid [2-(3,4-dibenzyloxy-5-oxo-2,5-dihydrofuran-2(R)-yl)-2(S)-hydroxyethyl] ester

: 400844-95-3
piperidine-3-carboxylic acid [2-(3,4-dibenzyloxy-5-oxo-2,5-dihydrofuran-2(R)-yl)-2(S)-hydroxyethyl] ester

Guidance literature:: With trifluoroacetic acid; In dichloromethane; for 2h;
DOI:10.1016/j.bmc.2004.07.043

Reference yield:

: 99663-32-8
(2R)-3,4-dibenzyloxy-2-[(1S)-1,2-dihydroxyethyl]-2H-furan-5-one

: 400844-95-3
piperidine-3-carboxylic acid [2-(3,4-dibenzyloxy-5-oxo-2,5-dihydrofuran-2(R)-yl)-2(S)-hydroxyethyl] ester

Guidance literature:: Multi-step reaction with 2 steps

1: 60 percent / DMAP; DCC / CH₂Cl₂ / 20 °C

2: 63 percent / CF₃COOH / CH₂Cl₂ / 2 h

With dmap; dicyclohexyl-carbodiimide; trifluoroacetic acid; In dichloromethane;
DOI:10.1016/j.bmc.2004.07.043