1-[(1S)-2-methoxy-2-oxo-1-phenylethyl] 4-methyl (2R)-2-benzyl-2-hydroxybutanedioate

Base Information

Chemical Name:1-[(1S)-2-methoxy-2-oxo-1-phenylethyl] 4-methyl (2R)-2-benzyl-2-hydroxybutanedioate
CAS No.:1137150-68-5
Molecular Formula:C₂₁H₂₂O₇
Molecular Weight:386.401
Hs Code.:

Synonyms:1-[(1S)-2-methoxy-2-oxo-1-phenylethyl] 4-methyl (2R)-2-benzyl-2-hydroxybutanedioate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-[(1S)-2-methoxy-2-oxo-1-phenylethyl] 4-methyl (2R)-2-benzyl-2-hydroxybutanedioate

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Technology Process of 1-[(1S)-2-methoxy-2-oxo-1-phenylethyl] 4-methyl (2R)-2-benzyl-2-hydroxybutanedioate

There total 1 articles about 1-[(1S)-2-methoxy-2-oxo-1-phenylethyl] 4-methyl (2R)-2-benzyl-2-hydroxybutanedioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 1137150-65-2
1-[(1S)-2-methoxy-2-oxo-1-phenylethyl] (2S)-2-(2-methoxy-2-oxoethyl)oxirane-2-carboxylate

: 591-51-5
phenyllithium

: 1137150-68-5
1-[(1S)-2-methoxy-2-oxo-1-phenylethyl] 4-methyl (2R)-2-benzyl-2-hydroxybutanedioate

Guidance literature:: phenyllithium; With copper(l) iodide; In diethyl ether; at -78 - -60 ℃; for 1.5h;

1-[(1S)-2-methoxy-2-oxo-1-phenylethyl] (2S)-2-(2-methoxy-2-oxoethyl)oxirane-2-carboxylate; In diethyl ether; at -78 ℃; for 2h;
DOI:10.1002/ejoc.200800935

Reference yield: 85.0%

: 1137150-68-5
1-[(1S)-2-methoxy-2-oxo-1-phenylethyl] 4-methyl (2R)-2-benzyl-2-hydroxybutanedioate

: 1137150-69-6
(2R)-2-benzyl-2-hydroxy-4-methoxy-4-oxobutanoic acid

Guidance literature:: With palladium on carbon; hydrogen; In ethyl acetate; at 20 ℃; for 24h; under 3750.38 Torr; Inert atmosphere;
DOI:10.1002/ejoc.200800935