4-(2,4-Dichlorphenyl)-1-<2-hydroxy-1-(methoxycarbonyl)-1-propenyl>-2,5-dimethyl-3-pyrrolcarbonsaeure-methylester

Base Information

• Chemical Name: 4-(2,4-Dichlorphenyl)-1-<2-hydroxy-1-(methoxycarbonyl)-1-propenyl>-2,5-dimethyl-3-pyrrolcarbonsaeure-methylester
• CAS No.: 98450-77-2
• Molecular Formula: C₁₉H₁₉Cl₂NO₅
• Molecular Weight: 412.27

Synonyms:4-(2,4-Dichlorphenyl)-1-<2-hydroxy-1-(methoxycarbonyl)-1-propenyl>-2,5-dimethyl-3-pyrrolcarbonsaeure-methylester

Chemical Property of 4-(2,4-Dichlorphenyl)-1-<2-hydroxy-1-(methoxycarbonyl)-1-propenyl>-2,5-dimethyl-3-pyrrolcarbonsaeure-methylester

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Technology Process of 4-(2,4-Dichlorphenyl)-1-<2-hydroxy-1-(methoxycarbonyl)-1-propenyl>-2,5-dimethyl-3-pyrrolcarbonsaeure-methylester

There total 1 articles about 4-(2,4-Dichlorphenyl)-1-<2-hydroxy-1-(methoxycarbonyl)-1-propenyl>-2,5-dimethyl-3-pyrrolcarbonsaeure-methylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

4-(2,4-Dichloro-phenyl)-5-[1-methoxycarbonyl-2-oxo-prop-(E)-ylideneamino]-2,5-dimethyl-4,5-dihydro-furan-3-carboxylic acid methyl ester (89730-49-4) → 4-(2,4-Dichlorphenyl)-1-<2-hydroxy-1-(methoxycarbonyl)-1-propenyl>-2,5-dimethyl-3-pyrrolcarbonsaeure-methylester (98450-77-2)

Guidance literature:

With hydrogen; platinum(IV) oxide; In methanol; Ambient temperature;

Reference yield: 86.0%

diazomethane (186581-53-3,908094-01-9,334-88-3) + 4-(2,4-Dichlorphenyl)-1-<2-hydroxy-1-(methoxycarbonyl)-1-propenyl>-2,5-dimethyl-3-pyrrolcarbonsaeure-methylester (98450-77-2) → 4-(2,4-Dichlorphenyl)-1-<2-methoxy-1-(methoxycarbonyl)-1-propenyl>-2,5-dimethyl-3-pyrrolcarbonsaeure-methylester (98450-71-6)

Guidance literature:

In diethyl ether; for 12h; Ambient temperature;

Reference yield: 54.0%

4-(2,4-Dichlorphenyl)-1-<2-hydroxy-1-(methoxycarbonyl)-1-propenyl>-2,5-dimethyl-3-pyrrolcarbonsaeure-methylester (98450-77-2) → 1-<1-Chlor-1-(methoxycarbonyl)-2-oxopropyl>-4-(2,4-dichlorphenyl)-2,5-dimethyl-3-pyrrolcarbonsaeure-methylester (98450-64-7)

Guidance literature:

With sodium hypochlorite; In chloroform; for 12h; Ambient temperature;

upstream raw materials:

4-(2,4-Dichloro-phenyl)-5-[1-methoxycarbonyl-2-oxo-prop-(E)-ylideneamino]-2,5-dimethyl-4,5-dihydro-furan-3-carboxylic acid methyl ester

Downstream raw materials:

4-(2,4-Dichlorphenyl)-1-<2-methoxy-1-(methoxycarbonyl)-1-propenyl>-2,5-dimethyl-3-pyrrolcarbonsaeure-methylester

1-<1-Chlor-1-(methoxycarbonyl)-2-oxopropyl>-4-(2,4-dichlorphenyl)-2,5-dimethyl-3-pyrrolcarbonsaeure-methylester

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