methyl 5-(aminomethyl)-2-{[2-[2-(methoxycarbonyl)phenyl]amino-5-(trifluoromethyl)phenyl]amino}-benzoate

Base Information

• Chemical Name: methyl 5-(aminomethyl)-2-{[2-[2-(methoxycarbonyl)phenyl]amino-5-(trifluoromethyl)phenyl]amino}-benzoate
• CAS No.: 640280-11-1
• Molecular Formula: C₂₄H₂₂F₃N₃O₄
• Molecular Weight: 473.452

Synonyms:methyl 5-(aminomethyl)-2-{[2-[2-(methoxycarbonyl)phenyl]amino-5-(trifluoromethyl)phenyl]amino}-benzoate

Chemical Property of methyl 5-(aminomethyl)-2-{[2-[2-(methoxycarbonyl)phenyl]amino-5-(trifluoromethyl)phenyl]amino}-benzoate

Chemical Property:

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Technology Process of methyl 5-(aminomethyl)-2-{[2-[2-(methoxycarbonyl)phenyl]amino-5-(trifluoromethyl)phenyl]amino}-benzoate

There total 1 articles about methyl 5-(aminomethyl)-2-{[2-[2-(methoxycarbonyl)phenyl]amino-5-(trifluoromethyl)phenyl]amino}-benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methyl 5-cyano-2-{[2-[2-(methoxycarbonyl)phenyl]amino-5-(trifluoromethyl)phenyl]amino}-benzoate (640280-10-0) → methyl 5-(aminomethyl)-2-{[2-[2-(methoxycarbonyl)phenyl]amino-5-(trifluoromethyl)phenyl]amino}-benzoate (640280-11-1)

Guidance literature:

With sodium tetrahydroborate; nickel dichloride; In tetrahydrofuran; methanol; at 0 - 20 ℃; for 2h;

Reference yield: 90.0%

methyl 5-(aminomethyl)-2-{[2-[2-(methoxycarbonyl)phenyl]amino-5-(trifluoromethyl)phenyl]amino}-benzoate (640280-11-1) + N-tert-butoxycarbonyl-L-phenylalanine (13734-34-4) → methyl 5-({[N-(tert-butoxycarbonyl)-L-phenylalanyl]amino}methyl)-2-{[2-{[2-(methoxycarbonyl) phenyl]amino}-5-(trifluoromethyl)phenyl]amino}benzoate (640280-15-5)

Guidance literature:

With N-cyclohexylcarbodiimide-N'-methyl polystyrene HL; In dichloromethane; at 20 ℃; for 24h; Polystyrene

Reference yield: 78.0%

methyl 5-(aminomethyl)-2-{[2-[2-(methoxycarbonyl)phenyl]amino-5-(trifluoromethyl)phenyl]amino}-benzoate (640280-11-1) + 3,5-dimethyl-1-pyrazolylformaminidium nitrate (38184-47-3) → methyl 5-({[amino(imino)methyl]amino}methyl)-2-{[2-{[2-(methoxycarbonyl)phenyl]amino}-5-(trifluoromethyl)phenyl]amino} benzoate (640280-18-8)

Guidance literature:

With triethylamine; In ethanol; at 20 ℃; for 4h;

upstream raw materials:

methyl 5-cyano-2-{[2-[2-(methoxycarbonyl)phenyl]amino-5-(trifluoromethyl)phenyl]amino}-benzoate

Downstream raw materials:

methyl 5-({[N-(tert-butoxycarbonyl)-L-phenylalanyl]amino}methyl)-2-{[2-{[2-(methoxycarbonyl) phenyl]amino}-5-(trifluoromethyl)phenyl]amino}benzoate

methyl 5-(aminomethyl)-2-{[2-[2-(methoxycarbonyl)phenyl]amino-5-(trifluoromethyl)phenyl]amino}-benzoate hydrochloride

methyl 5-({[amino(imino)methyl]amino}methyl)-2-{[2-{[2-(methoxycarbonyl)phenyl]amino}-5-(trifluoromethyl)phenyl]amino} benzoate

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