1-Cyclopentene-1-carbonylchloride, 5,5-dimethyl-

Base Information

Chemical Name:1-Cyclopentene-1-carbonylchloride, 5,5-dimethyl-
CAS No.:154222-76-1
Molecular Formula:C8H11 Cl O
Molecular Weight:158.62534
Hs Code.:
DSSTox Substance ID:DTXSID70445969
Wikidata:Q82264522
Mol file:154222-76-1.mol

Synonyms:154222-76-1;5,5-dimethylcyclopentene-1-carbonyl Chloride;1-Cyclopentene-1-carbonylchloride, 5,5-dimethyl-;1-Cyclopentene-1-carbonyl chloride, 5,5-dimethyl- (9CI);DTXSID70445969

Suppliers and Price of 1-Cyclopentene-1-carbonylchloride, 5,5-dimethyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 1 raw suppliers

Chemical Property of 1-Cyclopentene-1-carbonylchloride, 5,5-dimethyl-

Chemical Property:

PSA：17.07000
LogP:2.49820
XLogP3:3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:158.0498427
Heavy Atom Count:10
Complexity:191

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1(CCC=C1C(=O)Cl)C

Technology Process of 1-Cyclopentene-1-carbonylchloride, 5,5-dimethyl-

There total 4 articles about 1-Cyclopentene-1-carbonylchloride, 5,5-dimethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 154222-75-0
5,5-dimethyl-1-cyclopentene-1-carboxylic acid

: 154222-76-1
5,5-dimethyl-1-cyclopentene-1-carbonyl chloride

Guidance literature:: With thionyl chloride; for 1h; Heating;
DOI:10.3987/COM-93-6465

Reference yield:

: 4541-32-6
2,2-dimethylcyclopentanone

: 154222-76-1
5,5-dimethyl-1-cyclopentene-1-carbonyl chloride

Guidance literature:: Multi-step reaction with 4 steps

1: 95 percent / zinc iodide / benzene / 7.5 h / Ambient temperature

2: 76 percent / phosphorus oxychloride, pyridine / 30 h / 110 °C

3: 80 percent / KOH / bis-(2-hydroxy-ethyl) ether / 72 h / 120 °C

4: 81 percent / thionyl chloride / 1 h / Heating

With pyridine; potassium hydroxide; thionyl chloride; zinc(II) iodide; trichlorophosphate; In diethylene glycol; benzene;
DOI:10.3987/COM-93-6465

Reference yield:

: 154222-74-9
5,5-dimethyl-1-cyclopentene-1-carbonitrile

: 154222-76-1
5,5-dimethyl-1-cyclopentene-1-carbonyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / KOH / bis-(2-hydroxy-ethyl) ether / 72 h / 120 °C

2: 81 percent / thionyl chloride / 1 h / Heating

With potassium hydroxide; thionyl chloride; In diethylene glycol;
DOI:10.3987/COM-93-6465