cyclohexanone tert-butyldimethylsilyl methyl ketal

Base Information

Chemical Name:cyclohexanone tert-butyldimethylsilyl methyl ketal
CAS No.:120743-95-5
Molecular Formula:C₁₃H₂₈O₂Si
Molecular Weight:244.45
Hs Code.:

Synonyms:cyclohexanone tert-butyldimethylsilyl methyl ketal

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of cyclohexanone tert-butyldimethylsilyl methyl ketal

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Technology Process of cyclohexanone tert-butyldimethylsilyl methyl ketal

There total 3 articles about cyclohexanone tert-butyldimethylsilyl methyl ketal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 108534-51-6
4-((tert-butyldimethylsilyl)oxy)-4-methoxycyclohexa-2,5-dienone

: 120743-95-5
cyclohexanone tert-butyldimethylsilyl methyl ketal

Guidance literature:: Multi-step reaction with 3 steps

1: 99 percent / H₂ / 5percent Pd/C / ethanol / 1 h / 3102.9 Torr

2: methanol / 0.25 h

3: NaBH₄ / methanol / 0.03 h / Heating

With sodium tetrahydroborate; hydrogen; palladium on activated charcoal; In methanol; ethanol;
DOI:10.1021/jo00273a033

Reference yield:

: 120743-98-8
C₂₀H₃₄N₂O₄SSi

: 120743-95-5
cyclohexanone tert-butyldimethylsilyl methyl ketal

Guidance literature:: With sodium tetrahydroborate; In methanol; for 0.0333333h; Yield given; Heating;
DOI:10.1021/jo00273a033

Reference yield:

: 120743-94-4
1,4-cyclohexanedione tert-butyldimethylsilyl methyl ketal

: 120743-95-5
cyclohexanone tert-butyldimethylsilyl methyl ketal

Guidance literature:: Multi-step reaction with 2 steps

1: methanol / 0.25 h

2: NaBH₄ / methanol / 0.03 h / Heating

With sodium tetrahydroborate; In methanol;
DOI:10.1021/jo00273a033