bis[N-(3-t-butyl-5-methoxysalicylidene)anilinato]zirconium(IV) dichloride

Base Information

Chemical Name:bis[N-(3-t-butyl-5-methoxysalicylidene)anilinato]zirconium(IV) dichloride
CAS No.:215050-90-1
Molecular Formula:C₃₆H₄₀Cl₂N₂O₄Zr
Molecular Weight:726.855
Hs Code.:

Synonyms:bis[N-(3-t-butyl-5-methoxysalicylidene)anilinato]zirconium(IV) dichloride

Suppliers and Price of bis[N-(3-t-butyl-5-methoxysalicylidene)anilinato]zirconium(IV) dichloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of bis[N-(3-t-butyl-5-methoxysalicylidene)anilinato]zirconium(IV) dichloride

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of bis[N-(3-t-butyl-5-methoxysalicylidene)anilinato]zirconium(IV) dichloride

There total 1 articles about bis[N-(3-t-butyl-5-methoxysalicylidene)anilinato]zirconium(IV) dichloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 21959-01-3,125410-70-0,125410-71-1
zirconium tetrachloride bis(tetrahydrofuran) complex

: 215033-57-1
C₆H₂OCH₃C(CH₃)3OHCHN(C₆H₅)

: 215050-90-1
bis[N-(3-t-butyl-5-methoxysalicylidene)anilinato]zirconium(IV) dichloride

Guidance literature:: With n-butyllithium; In tetrahydrofuran; (Ar), ligand in THF at -78°C treated with n-butyllithium in hexane dropwise for 5 min, warmed to room temp., stirred for 2 h, treated dropwise with Zr complex at -78°C, warmed to room temp., stirred for15 h; concd.(vac.), stirred in CH2Cl2, filtered, washed (CH2Cl2), organic filtrate concd.(vac.), recrystd., elem. anal., NMR;
DOI:10.1016/S1381-1169(01)00050-4