dimethyl(3-phenyl-3-(4-(trifluoromethyl)phenoxy)propyl)sulfonium tetrafluoroborate

Base Information

• Chemical Name: dimethyl(3-phenyl-3-(4-(trifluoromethyl)phenoxy)propyl)sulfonium tetrafluoroborate
• CAS No.: 1425794-26-8
• Molecular Formula: BF₄*C₁₈H₂₀F₃OS
• Molecular Weight: 428.222
• Mol file: 1425794-26-8.mol

Synonyms:dimethyl(3-phenyl-3-(4-(trifluoromethyl)phenoxy)propyl)sulfonium tetrafluoroborate

Chemical Property of dimethyl(3-phenyl-3-(4-(trifluoromethyl)phenoxy)propyl)sulfonium tetrafluoroborate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of dimethyl(3-phenyl-3-(4-(trifluoromethyl)phenoxy)propyl)sulfonium tetrafluoroborate

There total 4 articles about dimethyl(3-phenyl-3-(4-(trifluoromethyl)phenoxy)propyl)sulfonium tetrafluoroborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 18.0%

methyl(3-phenyl-3-(4-(trifluoromethyl)phenoxy)propyl)sulfane (1425794-24-6) + trimethoxonium tetrafluoroborate (420-37-1) → dimethyl(3-phenyl-3-(4-(trifluoromethyl)phenoxy)propyl)sulfonium tetrafluoroborate (1425794-26-8)

Guidance literature:

In dichloromethane; at 20 ℃; Inert atmosphere;

Reference yield:

benzene (71-43-2,26181-88-4,54682-86-9,13967-78-7,174973-66-1) → dimethyl(3-phenyl-3-(4-(trifluoromethyl)phenoxy)propyl)sulfonium tetrafluoroborate (1425794-26-8)

Guidance literature:

Multi-step reaction with 4 steps

1.1: aluminum (III) chloride / dichloromethane / 0 - 20 °C / Inert atmosphere

2.1: sodium tetrahydroborate; ethanol / tetrahydrofuran / 0.25 h / Inert atmosphere

2.2: Inert atmosphere

3.1: sodium hydride / mineral oil; dimethyl sulfoxide / 0.75 h / 55 °C / Inert atmosphere

3.2: 1 h / 95 °C / Inert atmosphere

4.1: dichloromethane / 20 °C / Inert atmosphere

With aluminum (III) chloride; sodium tetrahydroborate; ethanol; sodium hydride; In tetrahydrofuran; dichloromethane; dimethyl sulfoxide; mineral oil;

Reference yield:

3-(methylsulfanyl)-1-phenylpropan-1-ol (39231-29-3) → dimethyl(3-phenyl-3-(4-(trifluoromethyl)phenoxy)propyl)sulfonium tetrafluoroborate (1425794-26-8)

Guidance literature:

Multi-step reaction with 2 steps

1.1: sodium hydride / mineral oil; dimethyl sulfoxide / 0.75 h / 55 °C / Inert atmosphere

1.2: 1 h / 95 °C / Inert atmosphere

2.1: dichloromethane / 20 °C / Inert atmosphere

With sodium hydride; In dichloromethane; dimethyl sulfoxide; mineral oil;

upstream raw materials:

benzene

3-chloropropiophenone

3-(methylsulfanyl)-1-phenylpropan-1-ol

methyl(3-phenyl-3-(4-(trifluoromethyl)phenoxy)propyl)sulfane